In this study, ZnO nanoparticles were prepared by a hydrothermal method with varying the reaction times, material ratios and reaction temperatures. The samples were characterized by scanning electron microscopy (SEM), transmission electron microscopy (TEM), X-ray Diffraction (XRD) and Fourier infrared spectroscopy (FTIR). It was shown that the material ratio significantly affected the structure and morphology of the synthesized ZnO nanoparticles, and then the uneven nano-octahedral structure, uniform nano-octahedral structure, nano-tubular structure, and nano-sheet structure could be obtained successively.
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