In this work, the pillaring of two layered niobium-based oxides (HNb O and HNbMoO ) with zirconia was investigated in detail. Two novel zirconia-pillared layered metal oxides, zirconia-pillared layered HNb O and zirconia-pillared layered HNbMoO , have been successfully prepared. Both pillared products exhibited a higher thermal stability exceeding 673 K.
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