Publications by authors named "Wojciech Pakiela"

This work covers a Mg-Zn-Ca-Pr alloy fabricated by a novel method of mechanical alloying and spark plasma sintering (SPS). Currently, magnesium alloys used as biomaterials are mostly commercial alloys without consideration of cytotoxicity from the perspective of biosafety. So far, the tribological and cytotoxic properties of Mg-Zn-Ca-Pr alloys have not been investigated.

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The article describes the results of the study on laser welding of armor plates with a nominal thickness of 3.0 mm. The plates were made of Armox 500T steel characterized by a hardness of up to 540 HB, a minimum yield strength of 1250 MPa, an ultimate strength of up to 1750 MPa, and an elongation A5 minimum of 8%.

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Titanium dioxide (TiO) thin films prepared by the sol-gel technique have been shown to be optically isotropic and, unlike the films obtained by competitive methods, do not exhibit measurable birefringence. A series of submicrometer-thin titanium dioxide films were prepared using the sol-gel technique and then thermally annealed at different temperatures. The samples were analyzed by spectroscopic ellipsometry using the Mueller matrix formalism, X-ray diffractometry and scanning electron microscopy.

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Denture fractures are a common problem in dental practice, and their repair is considered a first option to restore their functional properties. However, the inter-material resistance may become compromised. Typically, the bond between these materials weakens.

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Re-tightening the loosened dental implant abutment screw is an accepted procedure, however the evidence that such screw will hold sufficiently is weak. The purpose of this study was material analysis of lost dental implant abutment screws made of the TiAlV alloy from various manufacturers, which became lost due to unscrewing or damaged when checking if unscrewed; undamaged screws could be safely re-tightened. Among 13 failed screws retrieved from 10 cases, 10 screws were removed due to untightening and 3 were broken but without mechanical damage at the threads.

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While functioning in the oral cavity, denture soft linings (SL) are exposed to contact with the microbiota. Dentures can offer perfect conditions for the multiplication of pathogenic yeast-like fungi, resulting in rapid colonisation of the surface of the materials used. In vitro experiments have also shown that yeast may penetrate SL.

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Colonization of temporary denture soft linings and underlying tissues by yeast-like fungi is an important clinical problem due to the negative influence on the process of prosthetic treatment. Typical hygienic procedures are often insufficient to prevent fungal infections, so in this study, an antimicrobial filler (silver sodium hydrogen zirconium phosphate) was introduced into acrylic soft liner at concentrations of 1, 2, 4, 6, 8 and 10% (/). The effect of this modification on antifungal properties against , cytotoxicity, Shore A hardness, tensile strength and tensile bond strength, sorption and solubility was investigated, considering the recommended 30-day period of temporary soft lining use.

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The objective of this study was to formulate dip coatings, incorporating casein, NaOH, and nanocrystalline hydroxyapatite (nanoHAp), with self-healing properties for application on ZnMg3.2 wt.% alloy in the field of biomedical applications.

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This paper presents the results of research on a newly developed surface layer made by laser remelting the working surface of the Cu-ETP (CW004A, Electrolytic Tough Pitch) copper section insulator guide with Cr-Al powder. For the investigation, a fibre laser was used with relatively high power, reaching 4 kW, so as to ensure a high gradient of cooling rate for microstructure refinement. The microstructure of the transverse fracture of the layer (SEM) and the distribution of elements in the microareas (EDS) were investigated.

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The magnesium-based alloys produced by mechanical alloying (MA) are characterized by specific porosity, fine-grained structure, and isotropic properties. In addition, alloys containing magnesium, zinc, calcium, and the noble element gold are biocompatible, so they can be used for biomedical implants. The paper assesses selected mechanical properties and the structure of the MgZnCaAu as a potential biodegradable biomaterial.

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Zinc oxide layers on soda-lime glass substrates were fabricated using the sol-gel method and the dip-coating technique. Zinc acetate dihydrate was applied as the precursor, while diethanolamine as the stabilizing agent. This study aimed to determine what effect has the duration of the sol aging process on the properties of fabricated ZnO films.

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Yeast-like fungi such as () are the primary pathogenic microorganism in the oral cavity of denture wearers. The research available so far, conducted according to a protocol based on the exposure of specimens to a suspension and their cutting with water cooling, shows that hard polymethyl methacrylate (PMMA) prosthetic materials are not only surface colonized, but also penetrated by microorganisms in a short time. This justifies the hypothesis that exposure to a suspension of the strain causes the changes in mechanical properties due to surface colonization and/or penetration of the samples.

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The specific combinations of materials and dopants presented in this work have not been previously described. The main goal of the presented work was to prepare and compare the different properties of newly developed composite materials manufactured by sintering. The synthetic- (SHAP) or natural- (NHAP) hydroxyapatite serves as a matrix and was doped with: (i) organic: multiwalled carbon nanotubes (MWCNT), fullerenes C60, (ii) inorganic: Cu nanowires.

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This research aims to characterize and examine the microstructure and mechanical properties of the newly developed M789 steel, applied in additive manufacturing. The data presented herein will bring about a broader understanding of the processing−microstructure−property−performance relationships in this material based on its chemical composition and heat treatment. Samples were printed using the laser powder bed fusion (LPBF) process and then the solution was annealed at 1000 °C for 1 h, followed by aging at 500 °C for soaking times of 3, 6 and 9 h.

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Advanced High-Strength Steels (AHSSs) are one of the most rapidly developing group of Fe-based metallic materials. Their excellent combination of high strength, ductility and formability is due to their complex microstructure and strain-induced martensitic transformation of metastable retained austenite (RA), which favors extra ductility of the sheet steels. A deformation temperature is one of the most important factors affecting the phase transformation behavior in these Fe–C–Mn–Al–Si systems.

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In this paper, three commercial cermet powders, WC-Co-Cr, WC-Co and WC-CrC-Ni, were sprayed by the High Velocity Oxy Fuel (HVOF) method onto magnesium alloy AZ31 substrate. The coatings were investigated in terms of their microstructure, phase analysis and residual stress. The manufactured coatings were analyzed extensively using optical microscopy (OM), X-ray diffraction (XRD), scanning (SEM) and transmission electron microscopy (TEM).

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Crack-free binary SiO:TiO composite films with the refractive index of ~1.94 at wavelength 632.8 nm were fabricated on soda-lime glass substrates, using the sol-gel method and dip-coating technique.

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In the present study, two different cermet coatings, WC-CrC-Ni and CrC-NiCr, manufactured by the high-velocity oxy-fuel (HVOF) method were studied. They are labeled as follows: WC-CrC-Ni coating-WC and CrC-NiCr coating-CrC. These coatings were deposited onto a magnesium alloy (AZ31) substrate.

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The kinetics of ferritic transformation and the corresponding microstructural evolution in 0.17C-3.1Mn-1.

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In present work the CrC-NiCr coating was deposited on magnesium alloy substrate with high velocity oxygen fuel (HVOF) spraying. The microstructure of the samples has been characterized by means of electron microscopy, SEM and phase composition analysis carried out. The porosity of coatings has been also estimated.

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The work examines the effect of rhenium addition on the structure and properties of Cu-2Ni-1Si alloys. The aim of this work was to answer the question of how the addition of rhenium will affect the strengthening mechanisms of rhenium-modified, saturated, plastically deformed and aged Cu-2Ni-1Si alloys. How will this affect the crystallization process? What effect will it have on the properties? Scanning electron microscopy (SEM) and analysis of chemical composition in microareas (energy-dispersive X-ray spectroscopy, EDS), light microscopy, measurements of microhardness and conductivity of the alloys were used for the investigations.

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The thermal conditions in the molten pool during the laser surface melting of ductile cast iron EN-GJS-700-2 were estimated by using infrared thermography and thermocouple measurements. The thermal data were then correlated with the microstructure of the melted zone. Additionally, the thermodynamic calculations of a Fe-C-Si alloy system were performed to predict the solidification path of the melted zone.

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This paper presents the effects of laser treatment (fiber laser YLS-4000) on the microstructure and selected mechanical properties of the surface layer of AlMg (AlMg9) foundry alloy obtained by alloying with boron carbide (BC). The correlation between laser alloying process parameters and selected properties of the formed layer was discussed. The studies were supported by microstructural analysis of the remelted zone (RZ), heat affected zone (HAZ), undissolved carbide particles, substrate material, and precipitates formed during rapid solidification.

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Colonization of polymeric dental prosthetic materials by yeast-like fungi and the association of these microorganisms with complications occurring during prosthetic treatment are important clinical problems. In previously presented research, submicron inorganic particles of silver sodium hydrogen zirconium phosphate (S-P) were introduced into poly(methyl methacrylate) (PMMA) denture base material which allowed for obtaining the antimicrobial effect during a 90 day experiment. The aim of the present study was to investigate the flexural strength, impact strength, hardness, wear resistance, sorption, and solubility during three months of storage in distilled water.

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In the published article, "Properties of Experimental Dental Composites Containing Antibacterial Silver-Releasing Filler" [...

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