In this study, we present a new cadmium(II)-based two-dimensional coordination polymer [Cd (L)(NA)(HO)] (L = Iminol form of N-nicotinoyl glycinate, NA = nicotinate), , containing two linkers generated from N-nicotinoyl glycine. A comprehensive investigation was carried out during the synthesis of the coordination polymers by varying the reaction time interval and temperature, and it revealed the formation of three distinct phases, of which two phases were previously reported and one was a new compound (. The structure of compound was determined by single-crystal X-ray diffraction, and it shows a corrugated layer structure with hydrogen bond interactions leading to three-dimensional supramolecular arrangements.
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