Multifunctional hybrid films made from CoT3OTx4 and CoFeT2OT4 nanoparticles inside a poly 3-hydroxybutyrate matrix and study of their impact in methyl orange photodegradation.

This work aims to produce hybrid materials with potential applications in dye photodegradation. Therefore, hybrid films were obtained by incorporating cobalt (II, III) oxide (Co3O4) or cobalt ferrite (CoFe2O4) nanoparticles (NPs) with 18 ± 1.6 nm and 26 ± 1.

Antibacterial and Cytotoxic Study of Hybrid Films Based on Polypropylene and NiO or NiFeO Nanoparticles.

This study presents an in vitro analysis of the bactericidal and cytotoxic properties of hybrid films containing nickel oxide (NiO) and nickel ferrite (NiFeO) nanoparticles embedded in polypropylene (PP). The solvent casting method was used to synthesize films of PP, PP@NiO, and PP@NiFeO, which were characterized by different spectroscopic and microscopic techniques. The X-ray diffraction (XRD) patterns confirmed that the small crystallite sizes of NiO and NiFeO NPs were maintained even after they were incorporated into the PP matrix.

Analysis of the Physicochemical, Mechanical, and Electrochemical Parameters and Their Impact on the Internal and External SCC of Carbon Steel Pipelines.

The review presented herein is regarding the stress corrosion cracking (SCC) phenomena of carbon steel pipelines affected by the corrosive electrolytes that comes from external (E) and internal (I) environments, as well as the susceptibility and tensile stress on the SCC. Some useful tools are presented including essential aspects for determining and describing the E-SCC and I-SCC in oil and gas pipelines. Therefore, this study aims to present a comprehensive and critical review of a brief experimental summary, and a comparison of physicochemical, mechanical, and electrochemical data affecting external and internal SCC in carbon steel pipelines exposed to corrosive media have been conducted.

Atomic-Scale Investigation on the Evolution of Tio-Anatase Prepared by a Sonochemical Route and Treated with NaOH.

To date, the formation mechanisms of TiO, as well as its heterostructures, have not been clarified. Moreover, detailed research on the transition from a tetragonal anatase phase to the monoclinic phase of the TiO(B) phase and their interface structure has been quite limited until now. In the present study, we report on the sonochemical synthesis of TiO-anatase with a crystallite size of 5.

Intercalated Intermetallic Compounds AlTi and FeTi in Microrods and Microtubes Obtained by Invariant Reaction of Mechanically Milled System AlTiFe.

This paper reports the production of intermetallic microrods and microtubes from the decomposition of an intermetallic compound in an AlTiFe system. The intermetallic compound was obtained by mechanosynthesis of elemental powders of Al, Ti and Fe over 300 h at 400 rpm, sintering from compacted powder particles at 300 MPa per minute and at 900 °C for 3600 s in an argon atmosphere. The milled and sintered samples were analyzed by X-ray diffraction (XRD), scanning electron microscopy (SEM) and high-resolution transmission electron microscopy (HRTEM).

Ozone sensing based on palladium decorated carbon nanotubes.

Multiwall carbon nanotubes (MWCNTs) were easily and efficiently decorated with Pd nanoparticles through a vapor-phase impregnation-decomposition method starting from palladium acetylacetonates. The sensor device consisted on a film of sensitive material (MWCNTs-Pd) deposited by drop coating on platinum interdigitated electrodes on a SiO₂ substrate. The sensor exhibited a resistance change to ozone (O₃) with a response time of 60 s at different temperatures and the capability of detecting concentrations up to 20 ppb.

Microstructural characterization of chitosan and alginate films by microscopy techniques and texture image analysis.

The aim of this work is to characterize the microstructure of chitosan and alginate edible films by microscopy techniques and texture image analysis. Edible films were obtained by solution casting and solvent evaporation. The microscopy techniques used in this work were: light, environmental scanning electron and atomic force microscopy.

A comparative study of physical and chemical processes for removal of biomass in biofilters.

After 6 months of operation a long-term biofilter was stopped for two weeks and then it was started up again for a second experimental period of almost 1.3 years, with high toluene loads and submitted to several physical and chemical treatments in order to remove excess biomass that could affect the reactor's performance due to clogging, whose main effect is a high pressure drop. Elimination capacity and removal efficiency were determined after each treatment.