This study developed a method to simultaneously determine 73 multi-class pesticides in okra fruit using LC-MS/MS and GC-MS/MS. The sample was extracted with acetonitrile and subsequent clean-up through dispersive-SPE method. The quantification level of the technique was 0.
View Article and Find Full Text PDFThis study aimed to screen the bioactive compounds from Prosopis juliflora leaf supercritical fluid extract and to assess its antimicrobial properties. Supercritical carbon dioxide and Soxhlet methods were used for extraction. The extract was subjected to Gas Chromatography-Mass Spectrometer (GC-MS) and Fourier Transform Infrared for the characterization of the phyto-components.
View Article and Find Full Text PDFEnviron Sci Pollut Res Int
March 2023
This study aims to develop a chitosan-zinc oxide nano-adsorbent-coated sand (CZOCS) filter bed for getting rid of milk processing industry wastewater (MPIW) in a safe way. Chitosan zinc oxide nano-adsorbent (CZnO) of 88.35 ± 2.
View Article and Find Full Text PDFEnviron Sci Pollut Res Int
February 2023
Milk-processing industry effluent (MPIE) poses severe problems for aquatic and environmental systems, especially in the South Asian region. Therefore, its treatment is of great interest. This study deals with the investigation of chitosan titanium dioxide nanoadsorbent (CTiO) coated onto sand particles via calcination that are used to remove the emerging pollutants.
View Article and Find Full Text PDFFortified rice analogues were developed utilising the broken-rice fortified with selected micronutrients like iron, folic acid and Vitamin A. The purpose of this study was to investigate the feasibility of fortifying rice analogues with micronutrients and retention after extrusion and cooking. Cold extruder operated at 55 rpm screw speed and 1.
View Article and Find Full Text PDFDevelopment process of rice analogues by utilising the broken rice (BRF) and broken pigeonpea dhal (BPDF) flours together with water and sodium alginate as binding agent through extrusion was carried out. Two variable viz, BPDF (20, 30 and 40%) and moisture content (25, 30 and 35%) were controlled in the study to produce rice analogue resembling the raw rice. The optimum combination of flour mixture established for 30% BPDF and 30% water content with highest desirability of 0.
View Article and Find Full Text PDFThe study was carried out to know the quality of small grey donkey milk powder by spray dryer. Donkey milk powder moisture, fat, protein, carbohydrate and ash were 4.12 (d.
View Article and Find Full Text PDFAn analytical method in pomegranate whole fruits and arils was developed in LC-MS/MS and validated as per SANTE/12682/2019. Samples were extracted following acetonitrile-based modified QuEChERS protocol. The method was linear and the coefficient of determination ranged between 0.
View Article and Find Full Text PDFA method for simultaneous determination of carbendazim and tebuconazole residues in cabbage was developed and validated in LC-MS/MS. Samples were extracted and purified following the modified QuEChERS procedure, which enabled the elution of carbendazim and tebuconazole at 0.96 and 5.
View Article and Find Full Text PDFThe present investigation was focused to compare chitosan based nano-adsorbents (CZnO and CTiO) for efficient treatment of dairy industry wastewater using Response Surface Methodology (RSM) and Artificial Neural Network (ANN) models. The nano-adsorbents were synthesized using chemical precipitation method and characterized by using scanning electron microscope with elemental detection sensor (SEM-EDS) and atomic force microscope (AFM). Maximum %R (96.
View Article and Find Full Text PDFPigeonpea grains are important sources of vegetarian proteins. It is the paramount importance to check the pesticide residues due to their frequent use during production. The LC-MS/MS and GC-MS/MS analytical method was developed and validated for the simultaneous determination of 79 pesticide residues in pigeonpea.
View Article and Find Full Text PDFComposition, nutritional value and sensory characteristics of donkey milk of Indian small grey breed was analysed using AOAC and other standard methods. Fresh donkey milk had 90.63% (w.
View Article and Find Full Text PDFDhal recovery from three popular varieties of North Karnataka was studied using CFTRI mini dhal mill with five different treatments at three different levels. It was observed that Gulyal variety treated with mustard oil recorded maximum hulling efficiency (79.4%) and finished product (68.
View Article and Find Full Text PDFThe belt and drum type meat-bone separator was developed for small-scale fish processing and evaluated using Tilapia fish (Oreochromis mossambicus) in terms of capacity, yield, percentage yield, bone content, colour and power consumption. It consists of a perforated drum (3 mm), single phase electric motor, speed reduction gear box and drive system. The machine was evaluated using two food grade belt viz.
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