This work reports the synthesis and characterization of preceramic- and polymer-derived SiOC aerogels obtained from a commercial siloxane resin. The preceramic aerogels were obtained by ambient pressure drying (ambigels) and CO supercritical drying. Despite different drying processes, the final ceramic ambi/aerogels have very similar microstructural features in density, porosity, pore size, and specific surface area.
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