This study reports the influence of ZrO/β-TCP hybridization on the thermal, mechanical, and physical properties of polyamide 12 composites to be suited for bone replacement. Amount of 15 wt% of nano-ZrO along with 5,10,15,20 and 25 wt% of micro-β-TCP was compounded with polyamide 12 via a twin-screw extruder. The hybrid ZrO2/β-TCP filled polyamide 12 exhibited higher thermal, mechanical and physical properties in comparison to unfilled polyamide 12 at certain filler loading; which is attributed to the homogenous dispersion of ZrO/β-TCP fillers particle in polyamide 12 matrix.
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November 2018
Objective: To compare the mechanical and biological properties of newly developed hybrid ceramics filled and unfilled polyamide 12 (PA 12) for craniofacial reconstruction via a fused deposition modelling (FDM) framework.
Methods: 15wt% of zirconia (ZrO) as well as 30, 35, and 40wt% of beta-tricalcium phosphate (β-TCP) were compounded with PA 12, followed by the fabrication of filament feedstocks using a single screw extruder. The fabricated filament feedstocks were used to print the impact specimens.
Objectives: To determine the diffusion coefficient, water sorption and solubility of various types of restorative dental composites and to evaluate the effect of acidic media (orange juice and coke) on their characteristics.
Methods: Resin composite specimens (Filtek™ Z350, Spectrum(®) TPH(®)3 and Durafill(®) VS) were prepared in a stainless steel mold of 1mm thickness and 10mm diameter (n=5) and light-cured. All samples were dried at 37°C, immersed in media (distilled water, orange and coke) at 37°C and weighed at suitable time intervals (15, 35, 155, 320, 785, etc.