This study introduces a highly efficient and straightforward method for synthesizing gold nanoparticles (AuNPs) within a glucosamine/alginate (GluN/Alg) nanocomposite via an ionotropic gelation mechanism in aqueous environment. The resulting nanocomposite, AuNPs@GluN/Alg, underwent thorough characterization using UV-vis, EDX, FTIR, SEM, TEM, SAED, and XRD analyses. The spherical AuNPs exhibited uniform size with an average diameter of 10.
View Article and Find Full Text PDFIn this work, ZnO nanoplates and FeO nanospindles were successfully fabricated a simple hydrothermal method using inorganic salts as precursors. The ZnO/FeO hybrid was fabricated using a mechanical mixture of two different ZnO : FeO weight ratios to investigate the effect of weight ratio on catalytic properties. Scanning electron microscopy (SEM) and transmission electron microscopy (TEM) images showed that ZnO nanoplates (NPls) are about 20 nm thick with lateral dimensions of 100 × 200 nm, and FeO nanospindles (NSs) are about 500 nm long and 50 nm wide.
View Article and Find Full Text PDFIn recent years, smartphones have been integrated into rapid colorimetric sensors for heavy metal ions, but challenges persist in accuracy and efficiency. Our study introduces a novel approach to utilize biogenic gold nanoparticle (AuNP) sensors in conjunction with designing a lightbox with a color reference and machine learning for detection of Fe ions in water. AuNPs were synthesized using the aqueous extract of leaf as reductants and stabilizing agents.
View Article and Find Full Text PDFIn this study, we developed an endoscopic hyperspectral imaging (eHSI) system and evaluated its performance in analyzing tissues within tissue phantoms and orthotopic mouse pancreatic tumor models. Our custom-built eHSI system incorporated a liquid crystal tunable filter. To assess its tissue discrimination capabilities, we acquired images of tissue phantoms, distinguishing between fat and muscle regions.
View Article and Find Full Text PDFWe present the in situ synthesis of silver nanoparticles (AgNPs) through ionotropic gelation utilizing the biodegradable saccharides lactose (Lac) and alginate (Alg). The lactose reduced silver ions to form AgNPs. The crystallite structure of the nanocomposite AgNPs@Lac/Alg, with a mean size of 4-6 nm, was confirmed by analytical techniques.
View Article and Find Full Text PDFRecently, there have been publications on preparing hybrid materials between noble metal and semiconductor for applications in surface-enhanced Raman scattering (SERS) substrates to detect some toxic organic dyes. However, the use of cuprous oxide/silver (CuO/Ag) to measure the trace amounts of methyl orange (MO) has not been reported. Therefore, in this study, the trace level of MO in water solvent was determined using a SERS substrate based on CuO microcubes combined with silver nanoparticles (Ag NPs).
View Article and Find Full Text PDFDecorating two-dimensional (2D) nanomaterials with nanoparticles provides an effective method to integrate their physicochemical properties. In this work, we present the hydrothermal growth process of 2D zinc oxide nanoplates (ZnO NPls), then silver nanoparticles (AgNPs) were uniformly distributed on the surface of ZnO NPls through the reduction procedure of silver nitrate with sodium borohydride to create a metal-semiconductor hybrid. The amount of AgNPs on the ZnO NPls' surface was carefully controlled by varying the volume of silver nitrate (AgNO) solution.
View Article and Find Full Text PDFMicroplastics (MPs) are small (< 5 mm) plastic particles that are widely found in marine, freshwater, terrestrial and atmospheric environments. Due to their prevalence and persistence, MPs are considered an emerging contaminant of environmental concern. The separation and quantitation of MPs from freshwater sediments is a challenging and critical issue.
View Article and Find Full Text PDFWe successfully synthesized ZnSe nanoparticles (NPs) by using a hydrothermal method. Careful analyses of X-ray diffraction pattern and high-resolution transmission electron microscopy images showed that the synthesized ZnSe NPs with the size of ˜100 nm and sphere-like morphology crystallized in the zincblende/cubic structure (the F-43m space group). This was also confirmed based upon characteristic vibration modes recorded by using Raman scattering spectroscopy.
View Article and Find Full Text PDFRutile TiO₂ with highly active facets has attracted much attention owing to its enhanced activity during the photocatalytic degradation of pollutants such as pharmaceuticals in wastewater. However, it is difficult to obtain by controlling the synthetic conditions. This paper reports a simple hydrothermal synthesis of rutile TiO₂ nanorods with highly exposed {110} facets.
View Article and Find Full Text PDFACS Appl Mater Interfaces
March 2018
Amorphous molybdenum selenide nanopowder, obtained by refluxing Mo(CO) and Se precursors in dichlorobenzene, shows several structural and electrochemical similarities to the amorphous molybdenum sulfide analogue. The molybdenum selenide displays attractive catalytic properties for the hydrogen evolution reaction in water over a wide range of pH. In a pH 0 solution, it operates with a small onset overpotential of 125 mV and requires an overpotential of 270 mV for generating a catalytic current of 10 mA/cm.
View Article and Find Full Text PDFFishborne zoonotic trematode (FZT) parasites are a serious food safety problem in Asian countries because of their tradition of eating raw fish. In northern Vietnam, the prevalence of FZT metacercariae (MC) in wild-caught and cultured fish is quite high. The objective of this study was to assess the risk for acquiring these parasites from raw fish dishes prepared in restaurants.
View Article and Find Full Text PDFFish-borne zoonotic trematodes (FZT) pose a risk to human food safety and health and may cause substantial economic losses in the aquaculture industry. In Nghe An Province, Vietnam, low prevalence of FZT for fish farmers but high prevalence for fish indicate that reservoir hosts other than humans may play a role in sustaining transmission. To determine whether domestic animals may be reservoir hosts, we assessed prevalence and species composition of FZT infections in dogs, cats, and pigs in a fish-farming community in Vietnam.
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