BaCaTiO ceramics were successfully synthesized by a simple solid-state reaction method. This study examined the influence of sintering temperature on the structure, microstructure, dielectric properties and electrical behavior of the material. The XRD analysis reveals that the tetragonal phase (P4mm) is dominant in all the synthesized materials, with those sintered at = 1400 °C and = 1450 °C being single-phase, while others exhibit a minor orthorhombic phase (Pbnm).
View Article and Find Full Text PDFTh-containing superconducting high entropy system with the nominal composition (NbTa)[Formula: see text](MoWTh)[Formula: see text] was synthesized. Its structural and physical properties were investigated by X-ray diffraction, scanning electron microscopy, energy dispersive X-ray spectroscopy, specific heat, resistivity and magnetic measurements. Two main phases of alloy were observed: major bcc structure and minor fcc.
View Article and Find Full Text PDFActa Crystallogr B Struct Sci Cryst Eng Mater
August 2023
A series of BiLaFeO samples with 0.00 ≤ x ≤ 0.30 was synthesized by the sol-gel method.
View Article and Find Full Text PDFLi-ion batteries are widely used as energy storage devices due to their excellent electrochemical performance. The cubic LiLaZrO (c-LLZO) compound is regarded as a promising candidate as a solid-state electrolyte for lithium-ion batteries due to its high bulk Li-ion conductivity, excellent thermal performance, and chemical stability. The standard manufacturing procedure involves the high-temperature and lengthy annealing of powders.
View Article and Find Full Text PDFHypothesis: Fe(CO) was deposited on SBA-15 from gaseous phase and the adsorbed iron precursor was oxidized and hydrolyzed. We hypothesize that a novel method produces composites of unique and useful properties. The absence of sulfur and halides in the composites is of special importance with respect of their potential application as catalysts and catalyst supports.
View Article and Find Full Text PDFObjectives: The aim of the study was to analyze the perinatal outcome of twin gestations and estimate the influence of chorionicity on the outcome in a large cohort of twin pregnancies in Poland.
Material And Methods: A retrospective analysis of 465 twin deliveries in 6 Polish centers in 2012 was conducted. Baseline characteristics, the course of pregnancy and labor, as well as the neonatal outcome were analyzed in the study group and according to chorionicity.
Solid-state sintering method was used to prepare ceramic materials based on bismuth ferrite, i.e., (BiFeO3)1 - x -(BaTiO3) x and Bi1 - x Nd x FeO3 solid solutions and the Aurivillius Bi5Ti3FeO15 compound.
View Article and Find Full Text PDFIntroduction: Ultrasonography is used routinely during pregnancy to screen and detect fetal abnormalities. However, there are some conditions like anhydramnios (a prevalent state in renal agenesis) or maternal obesity that may limit the diagnostic accuracy of ultrasonography. Magnetic resonance imaging has proven to be useful when ultrasound alone is insufficient to make a correct diagnosis.
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