Publications by authors named "Tiago Jose Marques Fraga"

The global concern over water pollution caused by contaminants of emerging concern has been the subject of several studies due to the complexity of treatment. Here, the synthesis of a graphene oxide-based magnetic material (GO@FeO) produced according to a modified Hummers' method followed by a hydrothermal reaction was proposed; then, its application as a photocatalyst in clonazepam photo-Fenton degradation was investigated. Several characterization analyses were performed to analyze the structure, functionalization and magnetic properties of the composite.

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Unlabelled: In this work, biogas was synthesized from malt enriched-craft beer bagasse with the objective to generate clean energy. Thus, a kinetic model based on thermodynamic parameters was proposed to represent the process with coefficient determination () of 0.82.

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Marine shell wastes were thermally activated and characterized as aragonite and calcite phases and were used in the removal of synthetic anionic dyes, Bright Blue Acid (NB180) and Reactive Red 133 (RR133). Benefited marine shells were classified as low-cost (USD 0.33/g of adsorbent) in comparison with other reported materials.

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Sodium percarbonate (SPC, 2NaCO∙3HO), is a compound that can be used under multiple environmental applications. In this work, SPC was employed as oxidant in the treatment of soil contaminated with diesel oil. The soil samples were collected during the earthmoving stage of RNEST Oil Refinery (Petrobras), Brazil.

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Multilayer graphene oxide (mGO) was synthesized and functionalized via co-precipitation method to produce magnetic FeO-functionalized multilayer graphene oxide nanocomposite (MmGO). Photocatalytic properties of MmGO were investigated in the photodegradation of raw textile wastewater samples. Fourier-transformed infrared spectroscopy revealed Fe-O vibrations, characterized by the band shift from 636.

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Functionalized graphene and its derivatives have been subject of many recent studies investigating their use as scavenger of various industrial pollutants. Adsorption is a feasible treatment, which can employ a wide variety of materials as adsorbents. Additionally, graphene has been distinguished for its remarkable properties, such as mechanical resistance, flexibility and electric conductivity.

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Amino-functionalized multilayer graphene oxide (Am-nGO) has been synthesized and applied to remove the reactive drimaren red (DR) from aqueous solutions. Infrared spectroscopy evidenced amine and amide presence by peaks at 1579 cm and a band between 3300 and 3500 cm. Raman spectroscopy showed an increment in I/I ratio after amino-FeO-functionalization of nGO from 1.

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Malacoculture waste (Anomalocardia brasiliana) shellfish shells (ABSS) were evaluated as adsorbents of Nylosan Brilliant Blue (NBB) acid dye. The ABSS were thermally activated at 1,000 °C for 10 h and then characterized by Fourier-transform infrared spectroscopy, analysis of specific surface area (BET), X-ray diffraction (XRD), and scanning electron microscopy. Point of zero charge (PZC) analysis of ABSS verified pH 13.

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Graphene oxide (GO) was synthetized from graphite oxidation via the modified Hummers method. Afterwards, the GO was functionalized with diethylenetriamine (DETA) and FeCl to obtain the novel amino-iron oxide functionalized graphene (GO-NH-FeO). FTIR, XRD, SEM with EDX, and Raman spectroscopy were performed to characterize both GO and GO-NH-FeO.

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The residue generated in the aluminium cold lamination (TTR) was submitted to a direct burning and then it was calcined at 500°C. BET, FTIR, SEM with EDX and TGA techniques were performed to characterize the adsorbent before and after the adsorption. BET analysis showed that TTR specific surface area was 55.

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