Rare-earth-based nanomaterials with exceptional electrochemical properties can be obtained a simple, low-cost, environment-friendly citrate-gel-matrix approach. Owing to their high specific capacitance, strong conductivity, and electrochemical stability, gallium-based materials are capable of withstanding numerous charge-discharge cycles, thus extending the life cycle of a supercapacitor. This tunability enabled researchers to alter the morphology and composition of the electrode to enhance supercapacitor performance.
View Article and Find Full Text PDFDalton Trans
October 2023
Single-phase inorganic nanostructures with multiple applications are required for cost-effective, sustainable applications to save the environment from toxic activities. Nickel vanadate (NiVO), possessing three phases, such as NiVO, NiVO, and NiVO, acts as an effective electrode material and potential electrochemical sensors. Nickel vanadate phases (NiVO, NiVO, and NiVO) were synthesized through the gel-matrix technique, and their phase purity, crystallinity, morphology, optical properties, .
View Article and Find Full Text PDFA cutting-edge approach has been attempted in the present work to develop two stable phases of samarium gallium oxide as functional materials in the form of energy storage electrodes and photocatalysts. A novel samarium gallium oxide with two stable phases has been synthesized by the gel matrix method. Their crystallinity, phase purity, and surface morphology were studied using modern analytical instruments, , XRD, Raman spectra, FESEM, TEM, XPS, and UV-visible spectra.
View Article and Find Full Text PDFThe enticing features of metal molybdates make them an attractive candidate for energy storage systems. This report describes the synthesis of three distinct single-phase bismuth molybdates (BiMoO; α-BiMoO, β-BiMoO, and γ-BiMoO) using the gel matrix particle growth method and their application in high-performance asymmetric supercapacitors. The single phase and purity of the synthesized BiMoO particles were confirmed by X-ray diffraction (XRD) and further verified by Raman analysis.
View Article and Find Full Text PDFLead-free halide perovskites have gained attention in recent years as viable materials with more distinctive characteristics than conventional semiconductor materials. Lead-free CsBiI colloidal perovskite nanocrystal is chosen to eliminate its single-phase synthesis difficulty and implement the material in bioimaging applications. Nanostructured CsBiI perovskite composites were coated with a thin coating of SiO by an tetraethyl orthosilicate/(3-aminopropyl)trimethoxysilane injection growth method to enhance their stability in aqueous medium and biocompatibility.
View Article and Find Full Text PDFHerein, we report cellulose-based threads from Indian sacred Lotus () of the Nymphaceae family embellished with MoS nanosheets for its enhanced hydrophobic and antimicrobial properties. MoS nanosheets synthesized by a coprecipitation method using sodium molybdate dihydrate (NaMoO·2HO) and thioacetamide (CHCSNH) were used as a sourse for MoS particle growth with cellulose threads extracted from lotus peduncles. The size, crystallinity, and morphology of pure and MoS-coated fibers were studied using X-ray diffractometry (XRD) and scanning electron microscopy (SEM).
View Article and Find Full Text PDFErbium co-doped TiO2 /Ag catalysts are synthesized by using a simple, one-step solvothermal method and characterized by X-ray diffraction, field-emission scanning electron microscopy, transmission electron microscopy, Raman analysis, X-ray photoelectron spectroscopy, and diffuse reflectance spectroscopy. The catalysts exhibit anatase crystal structures with increased visible light absorption compared with pure TiO2 . Enhanced photocatalytic activity is observed with Er co-doped TiO2 /Ag nanocomposites for Rhodamine B degradation under visible light irradiation.
View Article and Find Full Text PDFCu2ZnSnS4 (CZTS) nanoparticles were synthesized by the precursor injection method using oleylamine as a solvent. Preliminary characterization indicated that the synthesized nanoparticles belonged to the kesterite structure with a bulged sphere-like morphology. Reduced graphene oxide (rGO) was synthesized by an improved Hummers method and was used for nanoparticle functionalization.
View Article and Find Full Text PDF