An ultrafast-responsive α-FeO/Fe(MoO) nanocomposite was developed for the detection of ethanol vapor. The α-FeO/Fe(MoO) nanocomposite was synthesized utilizing a green, normal-pressure, microwave-assisted method followed by an in situ solid-state reaction process with flower-like MoS as a unique precursor. The resulting α-FeO/Fe(MoO) composite presents a porous, agminated petal-like structure with α-FeO nanoparticles homogeneously attached to the surfaces of Fe(MoO) nanosheets.
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