Effect of customized bioactive glass in experimental composites on dentin bond strength after 12 months of aging.

Objectives: This study aimed to investigate the effect of a customized low-sodium bioactive glass (BG) fillers in experimental resin composites on their bond strength to dentin after 12 months of artificial aging. Specifically, it evaluated whether the bond strength was affected by different BG concentrations (0, 10, 20, 40 wt%) and artificial aging durations (1, 6, and 12 months).

Materials And Methods: Experimental composites were prepared with 10, 20, and 40 wt% of a customized low-sodium fluoride-containing BG.

Effect of Silane-Containing Adhesives on Repair Bond Strength between Fresh and Aged Composite Materials-A Pilot Study.

This study investigated the effects of different surface treatments and a silane-containing adhesive on the repair bond strength between fresh and aged resin composites. A total of 140 composite specimens were prepared and aged for 24 h or 4 months. Each group was subdivided into seven subgroups ( = 10) depending on the surface treatment (no surface treatment (NT), sandblasting (SAND), or Sof-lex coarse disc (DISC)) in combination with the use of the silane-containing adhesive ScotchBond Universal Plus (SBU) or an adhesive without silane Prime&Bond Universal (P&B).

Environmental implications of dental restorative materials on the zebrafish Danio rerio: Are dental chair drainage systems an emerging environmental threat?

This study aimed to evaluate the environmental impact of dental materials: commercial composite Tetric EvoCeram®, glass ionomer Equia Forte® HT Fil, laboratory-prepared composite, alkasite Cention® Forte, amalgam Amalcap® Plus, and samples from dental chair drainage systems (DCDS). Methacrylate monomers were detected in the eluates of experimental and commercials composites, and alkasite. In DCDS samples solely mercury was found at concentrations of 0.

Mechanical Properties of Alkasite Material with Different Curing Modes and Simulated Aging Conditions.

This study aimed to evaluate the micro-mechanical and macro-mechanical properties of self-cured and light-cured alkasite and to investigate how accelerated degradation in acidic, alkaline, and ethanol solutions affects the macro-mechanical properties of self-cured and light-cured alkasite. The specimens of the alkasite material (Cention Forte, Ivoclar Vivadent) were prepared according to the following three curing modes: (1) light-cured immediately, (2) light-cured after a 5-min delay, and (3) self-cured. Microhardness was tested before and after immersion in absolute ethanol to indirectly determine crosslink density, while flexural strength and flexural modulus were measured using a three-point bending test after accelerated aging in the following solutions: (1) lactic acid solution (pH = 4.

One-Year Evaluation of High-Power Rapid Curing on Dentin Bond Strength.

This study investigated the effect of 3 s light-curing with a high-power LED curing unit on the shear bond strength of bulk-fill composites. Four bulk-fill composites were bonded to dentin with a universal adhesive (Scotchbond Universal Plus): two materials designed for rapid curing (Tetric PowerFill and Tetric PowerFlow) and two controls (Filtek One Bulk Fill Restorative and SDR Plus Bulk Fill Flowable). The 4 mm composite layer was light-cured with Bluephase PowerCure for 20 s at 1000 mW/cm ("20 s") or for 3 s at 3000 mW/cm ("3 s").

Monowave vs. Polywave Light - Curing Units: Effect on Light Transmission of Composite without Alternative Photoinitiators.

Objective: The aim of this study was to compare the light transmission of monowave and polywave-curing devices by a bulk-fill composite containing only camphorquinone as a photoinitiator.

Materials And Methods: Three light-curing devices were used to cure bulk-fill composite QuiXfil: one monowave (Translux® Wave) and two polywave (VALO Cordless and Bluephase® PowerCure. The NIST-calibrated spectrometer (MARC Resin Calibrator, BlueLight Analytics Inc.

Influence of the Bracket Material on the Post-Cure Degree of Conversion of Resin-Based Orthodontic Adhesive Systems.

The aim of this study was to examine the influence of the orthodontic bracket material on the short-term and long-term post-cure development of the degree of conversion (DC) of resin-based orthodontic adhesive systems. Five commercially available materials characterized by different compositions and curing modes (light-curable or dual-curable) were tested under three different light curing conditions: without brackets (control group, CO), and in the presence of metal brackets (MB group) or ceramic brackets (CB group). Fourier-transform infrared spectroscopy was used to determine the post-cure DC development, both after "short-term" periods (2, 6, and 10 min) and "long-term" periods (1, 7, and 28 days).

Proposition of New Testing Procedure for the Mechanical Properties of Bulk-Fill Materials.

This study analysed flexural properties, microhardness, and the degree of conversion (DC) of five bulk-fill composites under clinically relevant conditions (4 mm thick specimens) in comparison to 2 mm specimens according to ISO 4049. Additionally, the effect of rapid polymerisation on 4 mm specimens was evaluated after accelerated aging. DC was measured using Fourier transform infrared spectrometry at 2 and 4 mm thick layers, while flexural properties and Vickers microhardness were tested using 16 × 2 × 2 mm or 16 × 2 × 4 mm specimens.

Water-Induced Changes in Experimental Resin Composites Functionalized with Conventional (45S5) and Customized Bioactive Glass.

The aim of the study was to evaluate microhardness, mass changes during 1-year water immersion, water sorption/solubility, and calcium phosphate precipitation of experimental composites functionalized with 5-40 wt% of two types of bioactive glass (BG): 45S5 or a customized low-sodium fluoride-containing formulation. Vickers microhardness was evaluated after simulated aging (water storage and thermocycling), water sorption and solubility were tested according to ISO 4049, and calcium phosphate precipitation was studied by scanning electron microscopy, energy dispersive X-ray spectroscopy, and Fourier-transform infrared spectroscopy. For the composites containing BG 45S5, a significant reduction in microhardness was observed with increasing BG amount.

Effect of polymerization mode on shrinkage kinetics and degree of conversion of dual-curing bulk-fill resin composites.

Objectives: To assess the behavior of dual-cure and conventional bulk-fill composite materials on real-time linear shrinkage, shrinkage stress, and degree of conversion.

Materials And Methods: Two dual-cure bulk-fill materials (Cention, Ivoclar Vivadent (with ion-releasing properties) and Fill-Up!, Coltene) and two conventional bulk-fill composites (Tetric PowerFill, Ivoclar Vivadent; SDR flow + , Dentsply Sirona) were compared to conventional reference materials (Ceram.x Spectra ST (HV), Dentsply Sirona; X-flow; Dentsply Sirona).

The Fluoride Ion Release from Ion-Releasing Dental Materials after Surface Loading by Topical Treatment with Sodium Fluoride Gel.

The study aimed to investigate the rechargeability of ion-releasing dental material specimens immersed in distilled water for 25 months, which depleted their ion-releasing ability. Four restorative dental materials (alkasite composite, giomer, glass-ionomer, and composite material) presented with 24 specimens were studied after topical treatment with a concentrated fluoride gel. The effect of resin coating on the ion uptake and release was investigated on additional 42 specimens of restorative dental materials with coatings.

Blue Laser for Polymerization of Bulk-Fill Composites: Influence on Polymerization Kinetics.

The objective of this study was to compare the polymerization kinetics of bulk-fill resin composites cured with a LED-curing device and a diode laser (449 nm). Three bulk-fill composites were light-cured with constant radiation exposure at 10 J/cm by varying radiant exitance and curing time. The following three light-curing protocols were used: (I) 3300 mW/cm for 3 s; (II) 2000 mW/cm for 5 s; and (III) 1000 mW/cm for 10 s.

Effect of Rapid Polymerization on Water Sorption and Solubility of Bulk-fill Composites.

Objectives: The aim of the study was to examine the impact of rapid high-intensity polymerization on water sorption and solubility of a new generation of bulk-fill composite materials.

Material And Methods: Five materials were tested: a conventional composite Filtek Z250 (3M, St. Paul, USA) and four bulk-fill composites, Filtek One Bulk Fill (3M), Tetric PowerFill (Ivoclar Vivadent, Schaan, Liechtenstein), Tetric PowerFlow (Ivoclar Vivadent), SDR Plus (Dentsply, Konstanz, Germany).

Improved Flexural Properties of Experimental Resin Composites Functionalized with a Customized Low-Sodium Bioactive Glass.

This study evaluated the flexural properties of an experimental composite series functionalized with 5-40 wt% of a low-Na F-containing bioactive glass (F-series) and compared it to another experimental composite series containing the same amounts of the conventional bioactive glass 45S5 (C-series). Flexural strength and modulus were evaluated using a three-point bending test. Degree of conversion was measured using Fourier-transform infrared spectroscopy.

Using Copper-Doped Mesoporous Bioactive Glass Nanospheres to Impart Anti-Bacterial Properties to Dental Composites.

Experimental dental resin composites containing copper-doped mesoporous bioactive glass nanospheres (Cu-MBGN) were developed to impart anti-bacterial properties. Increasing amounts of Cu-MBGN (0, 1, 5 and 10 wt%) were added to the BisGMA/TEGDMA resin matrix containing micro- and nano-fillers of inert glass, keeping the resin/filler ratio constant. Surface micromorphology and elemental analysis were performed to evaluate the homogeneous distribution of filler particles.

Post-Cure Development of the Degree of Conversion and Mechanical Properties of Dual-Curing Resin Cements.

This study investigated the effect of different curing conditions on the degree of conversion and mechanical properties of contemporary dual-curing resin cements. The material specimens were either light-cured directly, light-cured through a 1-mm lithium disilicate glass-ceramic layer, or self-cured. The degree of conversion was measured in 0.

Polymerization Kinetics and Development of Polymerization Shrinkage Stress in Rapid High-Intensity Light-Curing.

This study investigated polymerization kinetics, linear shrinkage, and shrinkage stress development for six contemporary composite materials of different viscosities cured using radiant exitances of 1100-2850 mW/cm. Real-time measurements of degree of conversion, linear shrinkage, and shrinkage stress were performed over 5 min using Fourier-transform infrared spectrometry, a custom-made linometer, and a custom-made stress analyzer, respectively. For most tested variables, the factor "material" had a higher effect size than the factor "curing protocol".

Impact of Copper-Doped Mesoporous Bioactive Glass Nanospheres on the Polymerisation Kinetics and Shrinkage Stress of Dental Resin Composites.

We embedded copper-doped mesoporous bioactive glass nanospheres (Cu-MBGN) with antibacterial and ion-releasing properties into experimental dental composites and investigated the effect of Cu-MBGN on the polymerisation properties. We prepared seven composites with a BisGMA/TEGDMA (60/40) matrix and 65 wt.% total filler content, added Cu-MBGN or a combination of Cu-MBGN and silanised silica to the silanised barium glass base, and examined nine parameters: light transmittance, degree of conversion (DC), maximum polymerisation rate (R), time to reach R, linear shrinkage, shrinkage stress (PSS), maximum PSS rate, time to reach maximum PSS rate, and depth of cure.

Long-Term Assessment of Contemporary Ion-Releasing Restorative Dental Materials.

The objective was to evaluate new commercially available ion-releasing restorative materials and compare them to established anti-cariogenic materials. Four materials were tested: alkasite Cention (Ivoclar Vivadent) in self-cure or light-cure mode, giomer Beautifil II (Shofu), conventional glass-ionomer Fuji IX (GC), and resin composite Tetric EvoCeram (Ivoclar Vivadent) as a control. Flexural strength, flexural modulus, and Weibull modulus were measured one day, three months, and after three months with accelerated aging in ethanol.

Effect of adhesive coating on calcium, phosphate, and fluoride release from experimental and commercial remineralizing dental restorative materials.

This study investigated the potential of adhesive coating for hindering the reactivity of ion-releasing dental restorative materials. Experimental composites were prepared by replacing 10 or 20 wt% of reinforcing fillers with two types of bioactive glass. A glass ionomer, a giomer, and an alkasite were used as representatives of commercial ion-releasing materials.

Aging-Dependent Changes in Mechanical Properties of the New Generation of Bulk-Fill Composites.

This study evaluated the behavior of a new generation of bulk-fill resin composites after prolonged exposure to an aqueous environment and accelerated aging in ethanol. Six bulk-fill materials were tested (Tetric PowerFill, Filtek One Bulk Fill Restorative, Tetric EvoCeram Bulk Fill, Fill-Up!, Tetric PowerFlow, SDR Plus Bulk Fill Flowable) and compared to two conventional reference materials (Tetric EvoCeram and Tetric EvoFlow). Flexural strength, modulus, and Weibull parameters were examined at three time points: 1 day, 30 days, and 30 days followed by ethanol immersion.

Ion release and hydroxyapatite precipitation of resin composites functionalized with two types of bioactive glass.

Objectives: To prepare experimental composites with bioactive glass (BG) and investigate their release of calcium (Ca), phosphate (PO), and fluoride (F), as well as pH changes and apatite precipitation after immersion.

Methods: Experimental composites were prepared with 0, 10, or 20 wt% of either BG 45S5 or a customized low-Na F-containing BG. Three commercial ion-releasing materials were used for reference.

Effect of Conventional Adhesive Application or Co-Curing Technique on Dentin Bond Strength.

The aim of this in vitro study was to assess the effect of two different adhesive application methods on shear dentin bond strength (ISO 29022) using three various adhesive systems. A mid-coronal section of 77 intact third human molars with fully developed apices was made to create flat bonding substrates. The materials used in the study were Excite F (Ivoclar Vivadent), Prime&Bond Universal (Dentsply Sirona) and G-Premio Bond (GC).

Experimental Bioactive Glass-Containing Composites and Commercial Restorative Materials: Anti-Demineralizing Protection of Dentin.

The purpose of this in vitro study was to investigate whether different types of experimental and commercial restorative dental materials can protect dentin against acid-induced softening. Experimental composites were prepared with a photocurable mixture of methacrylates and two types of bioactive glass (45S5 and a customized low-Na F-containing formulation). Human dentin samples were prepared from mid-coronal tooth slices and immersed in lactic acid solution (pH = 4.

Polymerization kinetics of experimental resin composites functionalized with conventional (45S5) and a customized low-sodium fluoride-containing bioactive glass.

This study aimed to investigate polymerization kinetics and curing light transmittance of two series of experimental dental resin composites filled with 0-40 wt% of either 45S5 bioactive glass (BG) or a customized low-Na F-containing BG. Polymerization kinetics in 0.1-mm and 2-mm thick layers were investigated through real-time degree of conversion measurements using a Fourier transform infrared (FTIR) spectrometer.