J Nanosci Nanotechnol
March 2021
We have studied the annealing behaviors of pure Al (Al-1050) and Al-Mg-Si alloy (Al-6061) with plate-type using a real-time synchrotron X-ray scattering in vacuum. At room temperature (RT), the crystal domain size of Al phase in the Al-Mg-Si alloy was small as 70 nm, compared to that in the pure Al, 142 nm. The crystal Al phase in the Al-Mg-Si alloy has more thermal stability than that in the pure Al.
View Article and Find Full Text PDFWe have studied the oxidation behaviors of aluminum (Al) nanopowders with different particle sizes using a real-time synchrotron X-ray scattering during annealing in air. The Al nanopowders with small particle size of 78 nm at room temperature (RT) were a single crystal. The surface of the nanopowders was first oxidized to amorphous Al oxide near 450 °C, and then crystallized to γ-Al₂O₃ phase at 550 °C.
View Article and Find Full Text PDFWe have studied the solid-phase sintering behaviors of Au nanopowders with different particle sizes using real-time synchrotron X-ray scattering and field-emission scanning electron microscopy (FESEM) experiments in air. Au powders with large particle size of 173 nm at room temperature showed a defect-free crystal domain size of 47 nm. Most of these powders showed multiple grains within the particle.
View Article and Find Full Text PDFJ Nanosci Nanotechnol
January 2020
We have studied the oxidation behaviors of Co, Cr, and Ni nanopowders for applications in biomedicine using a real-time synchrotron X-ray scattering in air. The Co nanopowders have a crystal domain size of 70 nm at room temperature (RT). The surface of the Co nanopowders was oxidized to CoO phase at RT.
View Article and Find Full Text PDFJ Nanosci Nanotechnol
November 2015
The phase transformation of Se/(Cu,In,Ga)/Mo/glass thin films during annealing in a vacuum on and off state was studied in a real-time synchrotron X-ray scattering experiment. The crystalline CIGS phase is a solid solution of crystalline CIS and CGS phases. The crystalline CIS phase was formed first at lower temperature.
View Article and Find Full Text PDFJ Nanosci Nanotechnol
November 2015
We have studied the process of new direct-spray roasting; SrCO3 powders were directly added into the 12FeCl2 x 4H2O solution first, and then α-Fe2O3 powders with the particle size of 210-620 nm was made after spray roasting in the low temperature of 400-700 degrees C. The direct-spray roasting enables us to get the uniform mixing of α-Fe2O3 and SrCO3 powders, and to lower the calcination temperature of Sr-ferrite, compared to that of the conventional dry method. Also, the magnetic properties of the powders made by direct-spray roasting are very higher than that made by the dry method.
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May 2013
The crystallization of Au/glass ultrathin films for surface plasmon resonance (SPR) biosensor has been studied using synchrotron X-ray scattering and field emission scanning electron microscope. In films thinner than 30 nm, crystallized Au grains with [111] preferred orientation were formed in the as-deposited amorphous precursor. In film with 58-nm thickness, however, Au (200) powder grains existed on top of the Au (111)-oriented grains near the interface.
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May 2013
Modified embedded atom method-molecular dynamics simulations have been performed to define the various growth facets at the interfaces of Au catalyzed-silicon nanowires (SiNWs). The interfacial growth facet of Au/SiNW on c-Si (111) surface has a single, planar interface, that grows parallel to the Si (111) planes. The interfacial growth facet on c-Si (211) surface has an asymmetrical, cone shape.
View Article and Find Full Text PDFThe use of a fiber optic quasi-distributed sensing technique for detecting the location and severity of water leakage is suggested. A novel fiber optic sensor probe is devised with a vessel of water absorption material called as water combination soil (WCS) located between two highly reflected connectors: one is a reference connector and the other is a sensing connector. In this study, the sensing output is calculated from the reflected light signals of the two connectors.
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April 2012
The crystallization of amorphous, Si-rich, Au28Si72/glass thin film was studied in real-time synchrotron X-ray scattering experiments. The amorphous film crystallizes first into Au and Si phases at a low temperature of 206 degrees C. At annealing temperatures above eutectic temperature (T(E) = 360 degrees C), the Au phase melts while the Si phase rapidly grows further.
View Article and Find Full Text PDFIn this paper, we derive the average bit error rate (BER) of subcarrier multiplexing (SCM)-based free space optics (FSO) systems using a dual-drive Mach-Zehnder modulator (DD-MZM) for optical single-sideband (OSSB) signals under atmospheric turbulence channels. In particular, we consider the third-order intermodulation (IM3), a significant performance degradation factor, in the case of high input signal power systems. The derived average BER, as a function of the input signal power and the scintillation index, is employed to determine the optimum number of SCM users upon the designing FSO systems.
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