High-throughput determination of grain size distributions by EBSD with low-discrepancy sampling.

Because microstructure plays an important role in the mechanical properties of structural materials, developing the capability to quantify microstructures rapidly is important to enabling high-throughput screening of structural materials. Electron backscatter diffraction (EBSD) is a common method for studying microstructures and extracting information such as grain size distributions (GSDs), but is not particularly fast and thus could be a bottleneck in high-throughput systems. One approach to accelerating EBSD is to reduce the number of points that must be scanned.

Determination of size distributions of non-spherical pores or particles from single x-ray phase contrast images.

Although x-ray tomography is commonly used to characterize the three-dimensional structure of materials, sometimes this is impractical due either to limited time for data collection (such as in rapidly-evolving systems) or the need to limit the radiation exposure of the sample. In such situations, it is desirable to extract as much information as possible from a more limited data set. In this paper, we describe how to extract the size distribution of non-spherical pores (or, equivalently, particles) from single x-ray phase contrast imaging (XPCI).

X-ray reflectivity measurement of interdiffusion in metallic multilayers during rapid heating.

A technique for measuring interdiffusion in multilayer materials during rapid heating using X-ray reflectivity is described. In this technique the sample is bent to achieve a range of incident angles simultaneously, and the scattered intensity is recorded on a fast high-dynamic-range mixed-mode pixel array detector. Heating of the multilayer is achieved by electrical resistive heating of the silicon substrate, monitored by an infrared pyrometer.

Universal slip dynamics in metallic glasses and granular matter - linking frictional weakening with inertial effects.

Slowly strained solids deform via intermittent slips that exhibit a material-independent critical size distribution. Here, by comparing two disparate systems - granular materials and bulk metallic glasses - we show evidence that not only the statistics of slips but also their dynamics are remarkably similar, i.e.

Universal Quake Statistics: From Compressed Nanocrystals to Earthquakes.

Slowly-compressed single crystals, bulk metallic glasses (BMGs), rocks, granular materials, and the earth all deform via intermittent slips or "quakes". We find that although these systems span 12 decades in length scale, they all show the same scaling behavior for their slip size distributions and other statistical properties. Remarkably, the size distributions follow the same power law multiplied with the same exponential cutoff.