Microwave Sintering of Alumina at 915 MHz: Modeling, Process Control, and Microstructure Distribution.

Microwave energy can be advantageously used for materials processing as it provides high heating rates and homogeneous temperature field distribution. These features are partly due to the large microwave penetration depth into dielectric materials which is, at room temperature, a few centimeters in most dielectric materials. However, up to now, this technology is not widely spread for high-temperature material processing applications (>1200 °C), because its reproducibly and ability to sinter large size samples (>30 cm) still needs to be improved.

Fast synthesis of nanocrystalline Mg2Si by microwave heating: a new route to nano-structured thermoelectric materials.

The ultra fast synthesis of nanocrystalline Mg(2)Si was carried out using microwave radiation. The elemental precursors were first milled together under dry conditions to get fine particles. The resulting mixture of powders of Mg and Si was cold pressed before being heated by microwave irradiation.

Sintering of CuO and ZnO in a single mode microwave cavity with shrinkage control.

A specific TE10m microwave cavity has been designed to follow-up the shrinkage during the microwave sintering of ceramics powders using an optical based position sensing device. The basic principle consists in measuring the distance from a laser source to the sample surface by means of a triangulation method. The spatial resolution device is around a few micrometers that enables to accurately measure the shrinkage versus time of a microwave irradiated sample.