An efficient modified QuEChERS procedure was established for the simultaneous determination of 37 pesticide residues in fresh and processed edible button mushroom by employing GC/ GC-MS and LC-MS/MS. The effectiveness, reliability and accuracy of the method were assessed through validation parameters such as linearity, LOD, LOQ, precision, accuracy, uncertainty, and matrix effect. The linearity calibration for all the selected pesticides at standard concentrations (0.
View Article and Find Full Text PDFEnviron Sci Pollut Res Int
November 2023
Liquid chromatography mass spectrometry (LC-MS)-based detection of flonicamid, imidacloprid and 6-chloronicotinic acid residues was validated and analysed in capsicum fruit, processed products and soil. The standard concentrations (0.0025 to 0.
View Article and Find Full Text PDFSpices such as paprika, curry, turmeric, dry chilli, and black pepper are grown in various geographic locations and widely used by consumers across the world. Pesticides applied during crop production practices could contaminate the produce, affecting the quality and posing a health risk for consumers. The complexity of the spice matrix and the wide range of target pesticides potentially present require special sample extraction and clean-up treatments to overcome matrix interference and ion suppression.
View Article and Find Full Text PDFA modified quick, easy, cheap, effective, rugged, and safe (QuEChERS) method was standardized for the analysis of cyantraniliprole residues in beetroot and beet top (Beta vulgaris ssp. vulgaris L.) using liquid chromatography-mass spectrometry/mass spectrometry.
View Article and Find Full Text PDFField and laboratory experiments were conducted to study the effect of simple decontamination methods and processing on imidacloprid, dimethoate, and emamectin benzoate residues in grapes and their processed products by liquid chromatography-mass spectrometry. Among the decontamination methods evaluated, washing with NaCl (2%) solution was effective for reducing imidacloprid (77.55%), dimethoate (83.
View Article and Find Full Text PDFDrought stress and pathogen infection simultaneously occur in the field. In this study, the interaction of these two stresses with chickpea, their individual and combined effect and the net impact on plant growth and yield traits were systematically assessed under field and confined pot experiments. The field experiments were conducted for four consecutive years from 2014-15 to 2017-18 at different locations of India.
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