Water as a Sustainable Leaching Agent for the Selective Leaching of Lithium from Spent Lithium-Ion Batteries.

The development of a sustainable recycling process for lithium from spent lithium-ion batteries is an essential step to reduce the environmental impact of batteries. So far, the industrial implementation of a recycling process for lithium has been hindered by low recycling efficiencies and impurities in the recycled material. The aim of this study is thus to develop an easy-to-implement recycling concept for the selective leaching of lithium from spent lithium-ion batteries with water as a sustainable leaching reagent.

Applying Material Science Principles to Chemical Stability: Modelling Solid State Autoxidation in Mifepristone Containing Different Degrees of Crystal Disorder.

Ball-milling and harsh manufacturing processes often generate crystal disorder which have practical implications on the physical and chemical stabilities of solid drugs during subsequent storage, transport, and handling. The impact of the physical state of solid drugs, containing different degrees/levels of crystal disorder, on their autoxidative stability under storage has not been widely investigated. This study investigates the impact of differing degrees of crystal disorder on the autoxidation of Mifepristone (MFP) to develop a predictive (semi-empirical) stability model.

Data-Driven Prediction of the Formation of Co-Amorphous Systems.

Co-amorphous systems (COAMS) have raised increasing interest in the pharmaceutical industry, since they combine the increased solubility and/or faster dissolution of amorphous forms with the stability of crystalline forms. However, the choice of the co-former is critical for the formation of a COAMS. While some models exist to predict the potential formation of COAMS, they often focus on a limited group of compounds.

High-Resolution Microstructure Characterization of Additively Manufactured X5CrNiCuNb17-4 Maraging Steel during Ex and In Situ Thermal Treatment.

Powder and selective laser melting (SLM) additively manufactured parts of X5CrNiCuNb17-4 maraging steel were systematically investigated by electron microscopy to understand the relationship between the properties of the powder grains and the microstructure of the printed parts. We prove that satellites, irregularities and superficial oxidation of powder particles can be transformed into an advantage through the formation of nanoscale (AlMnSiTiCr) oxides in the matrix during the printing process. The nano-oxides showed extensive stability in terms of size, spherical morphology, chemical composition and crystallographic disorder upon in situ heating in the scanning transmission electron microscope up to 950 °C.

Evolution of Microstructure and Texture in Laboratory- and Industrial-Scaled Production of Automotive Al-Sheets.

With the rising importance of aluminum sheets for automotive applications, the influence of microstructure and texture on mechanical properties and on forming behavior has gained re-increased interest in recent years. This paper provides an introduction to the topic and demonstrates the evolution of microstructure and texture in the standard alloys EN AW-5182 and EN AW-6016 for different processing scales. Moreover, strategies for texture and microstructure characterization of automotive Al-sheets are discussed.

Influence of Melt-Pool Stability in 3D Printing of NdFeB Magnets on Density and Magnetic Properties.

The current work presents the results of an investigation focused on the influence of process parameters on the melt-track stability and its consequence to the sample density printed out of NdFeB powder. Commercially available powder of Nd7.5Pr0.

Biotransformation of Scheelite CaWO by the Extreme Thermoacidophile : Tungsten-Microbial Interface.

The tungsten-microbial interactions and microbial bioprocessing of tungsten ores, which are still underexplored, are the focus of the current study. Here we show that the biotransformation of tungsten mineral scheelite performed by the extreme thermoacidophile leads to the breakage of scheelite structure and subsequent tungsten solubilization. Total soluble tungsten is significantly higher in cultures containing grown on scheelite than the abiotic control, indicating active bioleaching.

Microstructure Evolution in a 6082 Aluminium Alloy during Thermomechanical Treatment.

Thermomechanical treatments of age-hardenable wrought aluminium alloys provoke microstructural changes that involve the movement, arrangement, and annihilation of dislocations, the movement of boundaries, and the formation or dissolution of phases. Cold and hot compression tests are carried out using a Gleeble 3800 machine to produce flow data as well as deformed samples for metallography. Electron backscattered diffraction and light optical microscopy were used to characterise the microstructure after plastic deformation and heat treatments.