Spray Flame Synthesis and Multiscale Characterization of Carbon Black-Silica Hetero-Aggregates.

The increasing demand for lithium-ion batteries requires constant improvements in the areas of production and recycling to reduce their environmental impact. In this context, this work presents a method for structuring carbon black aggregates by adding colloidal silica via a spray flame with the goal of opening up more choices for polymeric binders. The main focus of this research lies in the multiscale characterization of the aggregate properties via small-angle X-ray scattering, analytical disc centrifugation and electron microscopy.

Particle and Phase Analysis of Combusted Iron Particles for Energy Storage and Release.

The combustion of metal fuels as energy carriers in a closed-cycle carbon-free process is a promising approach for reducing CO emissions in the energy sector. For a possible large-scale implementation, the influence of process conditions on particle properties and vice versa has to be well understood. In this study, the influence of different fuel-air equivalence ratios on particle morphology, size and degree of oxidation in an iron-air model burner is investigated by means of small- and wide-angle X-ray scattering, laser diffraction analysis and electron microscopy.