In this work, a hydrometallurgical process for the recycling of diamond core drilling crowns by means of aqua regia leaching and subsequent alkali leaching was investigated. This investigation continues a previous study in which nitric acid was used for the acid leaching phase. In the current study, higher tungsten recovery was achieved, reaching 98.
View Article and Find Full Text PDFElemental sulfur (S) is a corrosive sulfur compound which was found to be extremely reactive to silver, causing intensive silver sulfide (AgS) deposition on on-load tap changer (OLTC) contacts in power transformers. A highly selective adsorbent (HSA), called Tesla'Ssorb, for the removal of S from mineral insulating oils was prepared from raw material (RM) using the novel procedure. In this study, the adsorption properties of HSA for the removal of S from the oil were determined.
View Article and Find Full Text PDFIn this study, an environmentally sustainable process of crystal violet, congo red, methylene blue, brilliant green, Pb, Cd, and Zn ions adsorption from aqueous solutions onto amino-modified starch derivatives was investigated. The degree of substitution, elemental analysis, swelling capacity, solubility, and FTIR, XRD, and SEM techniques were used to characterize the adsorbents. The influence of pH, contact time, temperature, and initial concentration has been studied to optimize the adsorption conditions.
View Article and Find Full Text PDFThe aim of this research was the synthesis of silver nanoparticles (SPA- and SPR-AgNPs) using the aqueous extracts of the aerial (SPA) and the root (SPR) parts of the plant L., their characterization, reaction condition optimization, and evaluation of their biological and catalytic activity. UV-Vis spectroscopy, X-ray powder diffraction (XRPD), scanning electron microscopy with EDS analysis (SEM/EDS), and dynamic light scattering (DLS) analysis were utilized to characterize the nanoparticles, while Fourier transform infrared (FTIR) spectroscopy was used to detect some functional groups of compounds present in the plant extracts and nanoparticles.
View Article and Find Full Text PDFThe study's objective was to obtain silver nanoparticles (SVAgNP and FUAgNP) using aqueous extracts of and . The optimal conditions for nanoparticle synthesis were determined and obtained; nanoparticles were then characterized using UV-Vis, Fourier-transform infrared spectroscopy (FTIR), X-ray powder diffraction (XRD), Dynamic Light Scattering (DLS), Scanning Electron Microscopy with Energy Dispersive Spectroscopy (SEM/EDS). SVAgNP and FUAgNP possessed a crystalline structure with 48.
View Article and Find Full Text PDFHighly porous lignin-based microspheres, modified by magnetite nanoparticles, were used for the first time for the removal of selenate anions, Se(VI), from spiked and real water samples. The influence of experimental conditions: selenate concentration, adsorbent dosage and contact time on the adsorption capacity was investigated in a batch experimental mode. The FTIR, XRD, SEM techniques were used to analyze the structural and morphological properties of the native and exhausted adsorbent.
View Article and Find Full Text PDFThis study was designed to evaluate the optimal conditions for the eco-friendly synthesis of silver nanoparticles (AgNPs) using L. (Lythraceae) aqueous extracts and their potential application and safe use. AgNPs synthesized using aerial parts (LSA-AgNPs) and root extract (LSR-AgNPs) were characterized by UV-Vis spectrophotometry, Fourier transform infrared spectroscopy (FTIR), scanning electron microscopy (SEM/EDS), and X-ray powder diffraction (XRPD).
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