Synthetic incorporation of palladium-nickel bimetallic nanoparticles within mesoporous silica/silica nanoparticles as efficient and cheaper catalyst for both cationic and anionic dyes degradation.

Nickel-palladium bimetallic nanocrystallite supported mesoporous silica/silica nanoparticles (MSPs/MSNPs) made at a controlled ratio of Pd/Ni via organotrialkoxysilane mediated reduction of palladium cations are reported. The organotrialkoxysilane serve as a template for the stabilization and formation of bimetallic Pd-Ni nanocrystallite within MSPs/MSNPs that are characterized by TEM, EDX, HR-SEM, HR-MS, XRD, BET and Elemental mapping analysis, kinetic analysis for degradation of both cationic and anionic dyes, i.e.