Development of a SPE/GC-MS method for the determination of organophosphorus pesticides in food samples using syringe filters packed by GNP/MIL-101(Cr) nanocomposite.

In this study, we report the synthesis and application of a nanocomposite comprising metal-organic framework MIL-101(Cr) and graphene nanopowder (GNP) as a promising sorbent for the extraction of organophosphorus pesticides (OPPs) in juices, water, vegetables and honey samples. A syringe filter, for the first time, was used to host the synthesized nanocomposite and extract the OPPs followed by GC-MS analysis. Different characterization methods including XRD, FTIR, TGA, BET and SEM were employed to confirm the formation of studied nanocomposite.