Direct Imaging of Surface Melting on a Single Sn Nanoparticle.

Despite previous studies, understanding the fundamental mechanism of melting metal nanoparticles remains one of the major scientific challenges of nanoscience. Herein, the kinetics of melting of a single Sn nanoparticle was investigated using transmission electron microscopy heating techniques with a temperature step of up to 0.5 °C.

Effect of Size on the Formation of Solid Solutions in Ag-Cu Nanoparticles.

Modern technologies stimulate the quest for multicomponent nanosized materials with improved properties, which are ultimately defined by the atomic arrangement and interphase interactions in the nanomaterial. Here, we present the results of the experimental study of the formation of solid solutions in Ag-Cu nanoparticles in a wide size and temperature range using TEM techniques. The Ag-Cu nanoparticles with a eutectic ratio of components were formed on an amorphous carbon film by the physical vapor deposition technique.

Synthesis of Nanoparticles and Theoretical Model of Their Retention in Plasma of RF Capacitive Discharge with Vertically Arranged Electrodes in Acetylene.

In the present research, experiments on the formation and retention of nanoparticles (NPs) in the plasma of radio frequency (RF) capacitive discharge in acetylene were carried out with vertically positioned internal electrodes. It has been shown via SEM and TEM techniques that NPs found on the horizontal tube wall after the discharge operation have a spherical shape with a predominant diameter of approximately 400-600 nm. HRTEM analysis reveals their amorphous structure.