Nanocatalyst-Assisted Facile One-Pot Synthesis of Glycidol from Glycerol and Dimethyl Carbonate.

This paper reports the facile one-pot synthesis of glycidol via the transesterification of glycerol with dimethyl carbonate using KNO/AlO nanoparticles as supporting catalysts. KNO/AlO nanoparticles were prepared by the impregnation method. XRD and FT-IR analyses indicated an interaction between KNO and AlO that enabled the decomposition of KNO during the process and resulted in the formation of KAlO, the Al-O-K group, and KO.