Stable polymeric micelles have been demonstrated to serve as suitable templates for creating mesoporous metals. Herein, we report the utilization of a core-shell-corona type triblock copolymer of poly(styrene--2-vinylpyridine--ethylene oxide) and H₂PtCl₆·H₂O to synthesize large-sized mesoporous Pt particles. After formation of micelles with metal ions, the reduction process has been carried out by vapor infiltration of a reducing agent, 4-(Dimethylamino)benzaldehyde.
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