This work explores the thermal treatment of V/P/O catalyst precursors to achieve active and selective catalysts for the oxidation of -butane to maleic anhydride (MA) in a continuous-flow fixed-bed reactor. Vanadyl pyrophosphate (V, VPP), the key catalyst component, is produced together with suitable V vanadium orthophosphate (VOPO) allotropic forms by thermally treating vanadyl hydrogen phosphate hemihydrate (VHP) under various atmospheres and temperature ramps. The characterization conducted by using X-ray diffraction, Raman spectroscopy, and reaction testing allowed the identification of optimal conditions for active and selective catalysts.
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