Aiming to investigate the influence of pore property of mesoporous material on thermal degradation and fire behavior of polystyrene (PS), the ultrafine iron derivatives were uniformly grown on the interior wall of SBA-15 via the coordination-induced assembly by bioinspired polydopamine (PDA). The resultant SBA-15@PDA@Fe was verified by various characterizations with the dominant component of FeOOH. Compared with PS composites with SBA-15, PS composites with SBA-15@PDA@Fe revealed the notably divergent alteration in thermal and thermal-oxidation degradation behavior, which was determined by the changed pore property.
View Article and Find Full Text PDFMartensite steel is induced from pearlitic steel by a newly discovered method, which is completely different from the traditional route of quenching austenitic steel. Both experimental and theoretical studies demonstrate that Fe-C martensite forms by severe deformation at room temperature. The new mechanism identified here opens a paths to material-design strategies based on deformation-driven nanoscale phase transformations.
View Article and Find Full Text PDFWe have developed on the DIFFABS-SOLEIL beamline a biaxial tensile machine working in the synchrotron environment for in situ diffraction characterization of thin polycrystalline films mechanical response. The machine has been designed to test compliant substrates coated by the studied films under controlled, applied strain field. Technological challenges comprise the sample design including fixation of the substrate ends, the related generation of a uniform strain field in the studied (central) volume, and the operations from the beamline pilot.
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