Paper-TiO-AgO floating photocatalysts were produced under mild condition and their photocatalytic activity for the degradation of aromatic amine under sunlight stimulant was investigated. Characterizations by Raman, XRD, XPS, DRS and PL confirmed the presence of TiO and AgO, and the morphology of the appended TiO/AgO layer was probed by FE-SEM. The photocatalytic activity of the prepared samples was investigated by the degradation of aniline (AN) in water under simulated sun-light illumination and constrained conditions, i.
View Article and Find Full Text PDFA facile method to produce paper-TiO decorated with AgBr nanoparticles by a mild hydrothermal process at 140 °C was reported. The synthesis method was based on the immersion of the paper in a ready-made suspension of TiO/AgBr, comprising TiO sol solution prepared in acidic conditions and AgBr solution (10 M). A paper-TiO sample was prepared and used as reference.
View Article and Find Full Text PDFThe functionalization of cotton fabric with photoactive TiO-Ag-AgBr nanostructured layer has been successfully developed using a low temperature non-aqueous sol-gel route and aqueous suspension of AgBr. Evidence for the growth of TiO layer and the immobilization of AgBr nanoparticles have been confirmed by Raman, XRD and XPS. GSDR analysis revealed a strong absorption in the visible region brought by surface Plasmon resonance (SPR) of Ag nanocrystals generated at the surface of AgBr.
View Article and Find Full Text PDFCarbohydr Polym
November 2018
Aiming the degradation of harmful molecules under visible light, new photocatalytic systems were created. For this purpose, the surface of chitosan thin films was modified in heterogeneous phase via a simple and straightforward mild chemical process: chemisorption of silver ions followed by the synthesis in situ of TiO at low temperature (100 °C). A high photocatalytic activity under visible light was observed, leading to the degradation and/or mineralization of different organic products such as o-toluidine, salicylic acid and 4-aminomethyl benzoic acid.
View Article and Find Full Text PDFThin films of chitosan (CS) coated on glass substrates were used as support for the immobilization of nanostructures TiO/ZnS via a mild chemical process followed by a hydrothermal treatment at 90 °C. The preparation route involved the coating of the CS film on the glass substrate followed by the deposition of a thin layer of Ti(OBu) precursor and immersion in a solution of Zn(OCCH) and NaS. After a hydrothermal treatment at 90 °C, an even layer of TiO anatase decorated by ZnS nanorods was generated.
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