Herein, hydrogels based on starch from corn, sweet cassava and bitter cassava were prepared by a straightforward approach. The hydrogels were obtained by an oxidation process using the redox system KMnO/NaHSO which leads to the formation of carbonyl and carboxyl groups with minimum polymer hydrolysis. The resulting oxidized samples as well as the native starches were extensively characterized by scanning electron microscopy, thermogravimetric analysis and wide angle X-ray scattering, among others.
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