In this study, an iron oxyhydroxide nanocomposite with magnetic properties has been successfully synthesized. The quantification of the phases determined by Rietveld refinement has shown the presence of 74% of -FeOOH (akaganeite) and 26% of Fe₃O₄ (magnetite). TEM images show aggregates of around 5-15 nm Fe₃O₄ nanoparticles with cubic morphology and -FeOOH somatoids and nanorods with length and width of 100-200 nm and 10-50 nm, respectively.
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