The adsorption properties of microporous spherical carbon materials obtained from the resorcinol-formaldehyde resin, treated in a solvothermal reactor heated with microwaves and then subjected to carbonization, are presented. The potassium-based activation of carbon spheres was carried out in two ways: solution-based and solid-based methods. The effect of various factors, such as chemical agent selection, chemical activating agent content, and the temperature or time of activation, was investigated.
View Article and Find Full Text PDFIn this work, low-pressure synthesis of carbon spheres from resorcinol and formaldehyde using an autoclave is presented. The influence of reaction time and process temperature as well as the effect of potassium oxalate, an activator, on the morphology and CO adsorption properties was studied. The properties of materials produced at pressureless (atmospheric) conditions were compared with those synthesized under higher pressures.
View Article and Find Full Text PDFAn ultra-low percolation threshold electrically conductive polymer nanocomposite incorporating graphene into a polyhedral oligomeric silsesquioxane polycaprolactone (POSS-PCL/graphene) is described in this paper. Multilayer graphene flakes were homogeneously dispersed into POSS-PCL at 0.08, 0.
View Article and Find Full Text PDFThe oxidation of copper is a complicated process. Copper oxide develops two stable phases at room temperature and standard pressure (RTSP): cuprous oxide (Cu2O) and cupric oxide (CuO). Both phases have different optical and electrical characteristics that make them interesting for applications such as solar cells or resistive switching devices.
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