The potential for low cost, environmentally friendly and high rate energy storage has led to the study of anatase-TiO₂ as an electrode material in aqueous Al electrolytes. This paper describes the improved performance from an electrochemically treated composite TiO₂ electrode for use in aqueous Al-ion batteries. After application of the cathodic electrochemical treatment in 1 mol/dm³ KOH, Mott⁻Schottky analysis showed the treated electrode as having an increased electron density and an altered open circuit potential, which remained stable throughout cycling.
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