Inorganic layered compounds (2D-materials), particularly transition metal dichalcogenide (TMDC), are the focus of intensive research in recent years. Shortly after the discovery of carbon nanotubes (CNTs) in 1991, it was hypothesized that nanostructures of 2D-materials can also fold and seam forming, thereby nanotubes (NTs). Indeed, nanotubes (and fullerene-like nanoparticles) of WS and subsequently from MoS were reported shortly after CNT.
View Article and Find Full Text PDFMultiwall WS nanotubes have been synthesized from WO nanowhiskers in substantial amounts for more than a decade. The established growth model is based on the "surface-inward" mechanism, whereby the high-temperature reaction with HS starts on the nanowhisker surface, and the oxide-to-sulfide conversion progresses inward until hollow-core multiwall WS nanotubes are obtained. In the present work, an upgraded SEM μReactor with H and HS sources has been conceived to study the growth mechanism in detail.
View Article and Find Full Text PDFNanocomposite materials, integrating nanoscale additives into a polymer matrix, hold immense promise for their exceptional property amalgamation. This study delves into the fabrication and characterization of polyetherimide (PEI) nanocomposite strings fortified with multiwall WS nanotubes. The manufacturing process capitalizes on the preferential alignment of WS nanotubes along the string axis, corroborated by scanning electron microscopy (SEM).
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