Microplastics are a new type of pollutants that have attracted attention recently. However, there is limited research on the uptake of environmental microplastics by plants. In this study, scanning electron microscopy (SEM), micro-Raman spectroscopy, and Raman mapping were employed to identify and detect label-free micron-sized polystyrene (PS) microplastics accumulated in the roots and stems of maize (Zea mays L.
View Article and Find Full Text PDFSpectrochim Acta A Mol Biomol Spectrosc
March 2024
This study investigates the application of surface-enhanced Raman spectroscopy (SERS) in the diagnosis of liver cancer using Ag@SiO nanoparticles as SERS substrates. A SERS test was conducted on serum samples obtained from patients with liver cancer and healthy individuals. After repeated several times experiments, it was found that the best SERS spectrum was obtained when the volume ratio of serum to deionized water was 1:2.
View Article and Find Full Text PDFSpectrochim Acta A Mol Biomol Spectrosc
April 2023
Carbosulfan gets easily decomposed into carbofuran and 3-Hydroxy carbofuran in vegetables and forms harmful residues. To detect the residues of carbosulfan in vegetables (for example, cowpeas), a super-sensitive method of surface-enhanced Raman spectroscopy (SERS) was used in this work. Silver sol was prepared as the SERS substrate.
View Article and Find Full Text PDFNanoscale Res Lett
September 2022
TiO flower like nanomaterials (FLNMs) are fabricated a hydrothermal method and Ag nanoparticles (NPs) are deposited electron beam evaporation. Several biological pigments (CV, R6G and RhB) are selected as target molecules to investigate their surface enhanced Raman scattering (SERS) property. The results demonstrate ultrasensitivity and high reproducibility.
View Article and Find Full Text PDFLung cancer is a fatal tumor threatening human health. It is of great significance to explore a diagnostic method with wide application range, high specificity, and high sensitivity for the detection of lung cancer. In this study, data fusion and wavelet transform were used in combination with Fourier transform infrared (FTIR) spectroscopy and Raman spectroscopy to study the serum samples of patients with lung cancer and healthy people.
View Article and Find Full Text PDFAn ultrasensitive Ag-deposited TiO flower-like nanomaterial (FLNM) surface-enhanced Raman scattering (SERS)-active substrate is synthesized via a hydrothermal method, and Ag nanoparticles (NPs) are deposited through electron beam evaporation. Malachite green (MG), which is widely used in aquaculture, is employed to assess the surface-enhanced Raman scattering (SERS) properties of TiO/Ag FLNMs. They exhibit ultrasensitivity (limit of detection (LOD) of MG reaches 4.
View Article and Find Full Text PDFLung cancer is the leading cause of cancer-related death in the world. Early diagnosis has great significance for the survival of patients with lung cancer. In this paper, attenuated total reflectance Fourier transform infrared (ATR-FTIR) spectroscopy combined with chemometrics was used to study the serum samples from patients with lung cancer and healthy people.
View Article and Find Full Text PDFSpectrochim Acta A Mol Biomol Spectrosc
December 2021
Liver cancer is the most common fatal malignant tumor in the world. Early diagnosis of liver cancer can improve the survival rate of the patients with liver disease. In this paper, Fourier transform infrared (FTIR) spectroscopy combined with curve fitting and chemometrics was used to distinguish the serum from patients from that of healthy people.
View Article and Find Full Text PDFDeficiency of selenium (Se) will lead to malnutrition and decreased immune function of the body. There is a common phenomenon of Se deficiency in foods. In this study, different concentrations of sodium selenite (NaSeO) were applied to Moringa oleifera grownin soil.
View Article and Find Full Text PDFA systematic design idea for liquid-filled cylindrical zoom lenses with ideal imaging quality over a wide focal length range is introduced in detail. The PWC method is used to calculate the initial structure parameters of the zoom lenses, and the optical design software ZEMAX is used to eliminate the spherical aberration at different focal lengths. Lenses named SLCL-Doublet are finally designed, which are formed by a symmetric liquid-core cylindrical lens (SLCL) filled with variable refractive index (RI) liquid and a doublet cylindrical lens capable of significantly weakening the spherical aberration.
View Article and Find Full Text PDFA seed-mediated electroless deposition (SMED) approach for fabrication of large-area and uniform gold nanoparticle films as efficient and reproducible as surface-enhanced Raman scattering (SERS) substrates was presented. This approach involved a seeding pretreatment procedure and a subsequent growth step. The former referred to activation of polylysine-coated glass slides in gold seed solution, and the latter required a careful control of the reactant concentration and reaction time.
View Article and Find Full Text PDFMater Sci Eng C Mater Biol Appl
December 2018
A simple and rapid approach to synthesize monodisperse and biocompatible gold nanoparticles (AuNPs) employing dextran as a reducing and stabilizing agents at different reaction conditions was described. The obtained dextran-gold nanoparticles (Dex-AuNPs) were characterized by transmission electron microscopy (TEM), UV-Vis spectroscopy, Nuclear magnetic resonance (NMR) spectroscopy, Fourier transformer infrared (FTIR) spectroscopy and X-ray diffraction (XRD) analysis. The TEM examinations showed the resultant particles were 4-50 nm in size, monodispersity and uniform particle size distribution.
View Article and Find Full Text PDFSpectrochim Acta A Mol Biomol Spectrosc
February 2018
Guang Pu Xue Yu Guang Pu Fen Xi
August 2016
Fourier transform infrared spectroscopy, two-dimensional correlation infrared spectroscopy and principal component analysis were used to discriminate seven species of boletus belonging to the same genus. The results showed that the absorption bands of original spectra were similar, which were mainly composed of the absorption bands of protein and polysaccharides, but tiny differences were still observed at the position and intensities of peaks. Two-dimensional correlation infrared spectroscopy technology was applied to study the sample.
View Article and Find Full Text PDFGuang Pu Xue Yu Guang Pu Fen Xi
July 2016
Tri-step infrared spectroscopy method of Fourier transform infrared spectroscopy, second derivative infrared spectroscopy and two-dimensional correlation infrared spectroscopy was firstly used to discriminate six species of mushrooms belonging to the genus Lactarius and Russula. The absorption bands of the original spectrum were very similar, which were composed by protein and polysaccharides, but tiny differences were observed at the position, shape and absorption intensities of peaks. Second derivative infrared spectroscopy technology was applied to study 6 species of the samples, there were obvious differences in the range of 1 800~1 400 and 1 200~800 cm-1.
View Article and Find Full Text PDFGuang Pu Xue Yu Guang Pu Fen Xi
December 2014
Fourier transform infrared spectroscopy (FTIR) and inductively coupled plasma mass spectrometry (ICP-MS) were used to study six types of farmland soil from different areas. The FTIR results showed that the infrared spectra of soil were mainly composed of the absorption band of clay minerals, organic matter and inorganic salts, such as carbonate, phosphate, manganate and so on. The mineral atlas of six soil samples were all of montmorillonite type.
View Article and Find Full Text PDFGuang Pu Xue Yu Guang Pu Fen Xi
December 2013
Fourier transform infrared (FTIR) spectroscopy combined with principal component analysis (PCA) and hierarchical cluster analysis (HCA) were used to identify and classify bamboo leaves. FTIR spectra of fifty-four bamboo leaf samples belonging to six species were obtained. The results showed that the infrared spectra of bamboo leaves were similar, and mainly composed of the bands of polysaccharides, protein and lipids.
View Article and Find Full Text PDFGuang Pu Xue Yu Guang Pu Fen Xi
September 2013
Fourier transform infrared (FTIR) spectroscopy combined with hierarchical cluster analysis was used to study the influence of leaf senescence on magnoliaceae cluster. FTIR spectra of young, mature and old yellow leaves were obtained from 14 species trees belonging to the three magnoliaceae subtribes. Results showed that the infrared spectra of the three subtribes plant leaves were similar, only with minor differences in the absorption intensity of several peaks.
View Article and Find Full Text PDFGuang Pu Xue Yu Guang Pu Fen Xi
February 2013
In order to investigate plant physiological process of leaf senescence and aging, Fourier transform infrared (FTIR) spectroscopy was used to study the young, mature, and old yellow leaves from seven species of evergreen trees. The spectra of the leaves from different growing period are different in the region of 1 800-700 cm(-1). The absorption ratios A1 070/A2 927, A1 070/A1 160 were used to evaluate the relative changes of polysaccharides, and A1 318/A2 922 was used to estimate the change of calcium oxalate during leaf senescence.
View Article and Find Full Text PDFGuang Pu Xue Yu Guang Pu Fen Xi
September 2012
Fourier transform infrared Spectroscopy (FTIR) was used to study healthy and diseased leaves of rice, corn, and broad bean. The results show that the infrared spectra of the leaves are mainly composed of the absorption bands of proteins and polysaccharide. The spectra are similar, but the differences were observed in the peak positions, shapes, and absorption ratios.
View Article and Find Full Text PDFIn the present paper, broad bean rust, fusarium rhizome rot, broad bean zonate spot, yellow leaf curl virus and normal leaves were studied using Fourier transform infrared spectroscopy combined with chemometrics. The results show that the spectra of samples were similar, only with minor differences in absorption intensity of several peaks. Second derivative analyses show that the significant difference of all samples was in the range of 1200-700 cm(-1).
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