Surface Roughening Behavior and Mechanism in Aluminum Alloy Under Tensile Deformation.

Surface roughening (SR) has been found to occur in solid solution 2219 aluminum alloy under tensile deformation, which will deteriorate its surface quality. To make a precise study of the surface roughening (SR) behavior and mechanism, the surface morphology of annealed and solid solution 2219 aluminum alloy was compared and crystal plasticity finite element (CPFE) simulation was carried out in this study. Thereinto, representative volume element (RVE) models of polycrystals were established according to the initial grain morphology measured by electron backscatter diffraction (EBSD).

Quantification ethyl carbamate in wines using reaction-assisted-extraction with 9-xanthydrol and detection by heart-cutting multidimensional gas chromatography-mass spectrometry.

9-Xanthydrol was introduced as an assisted-extraction-reagent to quantify ethyl carbamate (EC) in wines by heart-cutting multidimensional gas chromatography coupled with mass spectrometry (MDGC-MS). 9-Xanthydrol could help to increase the extraction efficiency, because it could react with ethyl carbamate to form the low-polar product, which facilitated the transfer of ethyl carbamate into organic phase. Then the reaction product was decomposed in high temperature, so ethyl carbamate could be obtained again in injector port.