Atomically resolved scanning tunneling microscope (STM) capable of in situ rotation in a narrow magnet bore has become a long-awaited but challenging technique in the field of strong correlation studies since it can introduce the orientation of the strong magnetic field as a control parameter. This article presents the design and functionality of a piezoelectrically driven rotatable STM (RSTM), operating within a 12 T cryogen-free magnet and achieving a base temperature below 1.8 K, along with spectroscopic capabilities.
View Article and Find Full Text PDFThe electronic orders in kagome materials have emerged as a fertile platform for studying exotic quantum states, and their intertwining with the unique kagome lattice geometry remains elusive. While various unconventional charge orders with broken symmetry is observed, the influence of kagome symmetry on magnetic order has so far not been directly observed. Here, using a high-resolution magnetic force microscopy, it is, for the first time, observed a new lattice form of noncollinear spin textures in the kagome ferromagnet in zero magnetic field.
View Article and Find Full Text PDFScanning tunneling microscope (STM) is a renowned scientific tool for obtaining high-resolution atomic images of materials. Herein, we present an innovative design of the scanning unit with a compact yet powerful inertial piezoelectric motor inspired by the Spider Drive motor principle. The scanning unit mainly consists of a small 9 mm long piezoelectric tube scanner (PTS), one end of which is coaxially connected to the main sapphire body of the STM.
View Article and Find Full Text PDFThe high resolution of a scanning tunneling microscope (STM) relies on the stability of its scan unit. In this study, we present an isolated scan unit featuring non-magnetic design and ultra-high stability, as well as bidirectional movement capability. Different types of piezoelectric motors can be incorporated into the scan unit to create a highly stable STM.
View Article and Find Full Text PDFLow-temperature scanning tunneling microscopy and spectroscopy (STM/S) help to better understand the fundamental physics of condensed matter. We present an ultracompact STM within a Φ 10 piezo tube in a 20 T superconducting magnet. The carefully cut piezo tube contains the STM's coarse-positioning assembly.
View Article and Find Full Text PDFWe present the design and performance of a novel scanning tunnelling microscope (STM) operating in a cryogen-free superconducting magnet. Our home-built STM head is compact (51.5 mm long and 20 mm in diameter) and has a single arm that provides complete openness in the scanning area between the tip and sample.
View Article and Find Full Text PDFMost known two-dimensional magnets exhibit a high sensitivity to air, making direct characterization of their domain textures technically challenging. Herein, we report on the construction and performance of a glovebox-assisted magnetic force microscope (MFM) operating in a cryogen-free magnet, realizing imaging of the intrinsic magnetic structure of water and oxygen-sensitive materials. It features a compact tubular probe for a 50 mm-diameter variable temperature insert installed in a 12 T cryogen-free magnet.
View Article and Find Full Text PDFWe present a mechanism for directly positioning the tip over a micron-size sample by tracking the trajectory of the tip and tip shadow. A bilayer graphene sheet identified by Raman spectroscopy with a lateral size of 20 μm × 50 μm was transferred on the surface of shaped gold electrodes, on which it will be rapidly captured by a homebuilt scanning tunneling microscopy (STM) with the help of an optical microscope. Using the improved line-based imaging mode, atomic-resolution images featuring a hexagonal lattice structure on the bilayer graphene sheet were obtained by our positioning-capable STM.
View Article and Find Full Text PDFThe reversible transformation of a nanohelix is one of the most exquisite and important phenomena in nature. However, nanomaterials usually fail to twist into helical crystals. Considering the irreversibility of the previously studied twisting forces, the reverse process (untwisting) is more difficult to achieve, let alone the retwisting of the untwisted crystalline nanohelices.
View Article and Find Full Text PDFSpectroscopic-imaging scanning tunnelling microscope (SI-STM) in a water-cooled magnet (WM) at low temperature has long been desirable in the condensed matter physics area since it is crucial for addressing various scientific problems, such as the behaviour of Cooper electrons crossing Hc2 in a high-temperature superconductor. Here we report on the construction and performance of the first atomically resolved cryogenic SI-STM in a WM. It operates at low temperatures of down to 1.
View Article and Find Full Text PDFWe present the first nonmetallic scanning tunneling microscope (STM) featuring an ultra-stable tip-sample mechanical loop and capable of atomic-resolution imaging within a 12 T magnetic field that could be either perpendicular or parallel to the sample surface. This is also the first STM with an ultra-stable tip-sample mechanical loop but without a standalone scanner. The STM head is constructed only with two parts: an improved spider-drive motor and a zirconia tip holder.
View Article and Find Full Text PDFScanning tunneling microscopes (STMs) that work in ultra-high vacuum and low temperatures are commonly used in condensed matter physics, but an STM that works in a high magnetic field to image chemical molecules and active biomolecules in solution has never been reported. Here, we present a liquid-phase STM for use in a 10 T cryogen-free superconducting magnet. The STM head is mainly constructed with two piezoelectric tubes.
View Article and Find Full Text PDFTopologically protected magnetic "whirls" such as skyrmions in antiferromagnetic materials have recently attracted extensive interest due to their nontrivial band topology and potential application in antiferromagnetic spintronics. However, room-temperature skyrmions in natural metallic antiferromagnetic materials with merit of probable convenient electrical manipulation have not been reported. Here, room-temperature skyrmions are realized in a non-collinear antiferromagnet, Mn Sn, capped with a Pt overlayer.
View Article and Find Full Text PDFMicromachines (Basel)
February 2023
Scanning tunneling microscopy (STM) can image material surfaces with atomic resolution, making it a useful tool in the areas of physics and materials. Many materials are synthesized at micron size, especially few-layer materials. Limited by their complex structure, very few STMs are capable of directly positioning and imaging a micron-sized sample with atomic resolution.
View Article and Find Full Text PDFThe Annual Conference and International Conference of the Chinese Association of Micro-NanoTechnology is a comprehensive, cross-disciplinary, high-level academic conference that has been held annually since 1994 and has become an important academic event in the field of micro- and nanotechnology [...
View Article and Find Full Text PDFWe present the design and construction of a nonmetallic tip-sample mechanical loop featured Scanning Tunneling Microscope (STM) that operates in a 22 T water-cooled magnet at a low temperature of l.8 K. The STM head mainly consists of a spider-drive motor, stand-alone scanner, moveable sapphire sample holder, and sapphire frame.
View Article and Find Full Text PDFMicromachines (Basel)
November 2022
Magnetic Force Microscopy (MFM) is among the best techniques for examining and assessing local magnetic characteristics in surface structures at scales and sizes. It may be viewed as a unique way to operate atomic force microscopy with a ferromagnetic tip. The enhancement of magnetic signal resolution, the utilization of external fields during measurement, and quantitative data analysis are now the main areas of MFM development.
View Article and Find Full Text PDFWe present a two-degree-of-freedom piezoelectric motor, which is driven by a simple cross-shaped piezo unit. Here, not only the structure of high novelty and simplicity but also the working principle is new. The cross-shaped piezo unit is sandwiched between top and bottom guiding plates with roughly equal pressing forces applied between the four free ends of the piezo unit and the plates.
View Article and Find Full Text PDFThe high-bandwidth preamplifier is a vital component designed to increase the scanning speed of a high-speed scanning tunneling microscope (STM). However, the bandwidth is limited not only by the characteristic GΩ feedback resistor R but also by the characteristic unity-gain-stable operational amplifier (UGS-OPA) in the STM preamplifier. Here, we report that paralleling a resistor with the tunneling junction (PRTJ) can break both limitations.
View Article and Find Full Text PDFJ Magn Reson Imaging
June 2021
Magnetic resonance imaging (MRI) of 7 T and higher can provide superior image resolution and capability. Clinical tests have been performed in 9.4 T MRI, and 21.
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