Structurally Modulated NiV-LDH with CdMoSe-Quantum Dots: Unlocking the Active Centers at S-Scheme Heterojunctions for Stimulating Photocatalytic HO Production and H Evolution.

Designing and accumulating quantum dots (QD) onto layered double hydroxide (LDH) for the photocatalytic production of H and HO is a formidable task. Here, we intended the synthesis procedure of CdMoSe-QD (CMS)-incorporated NiV-LDH (NV) through a facile in situ reflux method and explored the photocatalytic activities of the CMS/NV (CNV) heterostructure. CNV-1 exhibits a large interface contact area and assures excellent interfacial charge transfer ability.