This study explores the characteristics and potential engineering applications of Cu-Al-Mn and Cu-Al-Be-Mn shape memory alloys (SMAs). The research investigates the chemical composition, transformation temperatures, and mechanical properties of these SMAs when incorporated into Al metal matrix composites (MMCs). It was found that the addition of Mn and Be, has a significant impact on the performance of Cu-Al alloys.
View Article and Find Full Text PDFThis present research aimed to investigate the novel applications of synthesized La doped CuFeO nanomaterial (LCF NMs) using renewable bio-fuel (Aegle Marmelos extract) by combustion process. The sensor applications were accomplished by modified electrode using LCF NMs with graphite powder and examined its excellent sensing action towards heavy metal (Lead content) and drug chemical (Paracetamol) substances. The thermodynamics of redox potential and super-capacitor behavior of LCF NMs were investigated through Cyclic Voltametric (CV) and Electrochemical Impedance Spectral (EIS) methods under specific conditions at scan rate of 1 to 5 mV/s.
View Article and Find Full Text PDFSpectrochim Acta A Mol Biomol Spectrosc
November 2023
The Europium activated (1-9 mol %) Zirconium Titanate nanoparticles (NPs) have been synthesized by the green solution combustion method using Aloe Vera gel extract as a reducing agent, followed by the calcination at 720 °C for 3hrs. All the synthesized samples crystallize in a pure orthorhombic crystal structure with the space group of Pbcn. The surface and bulk morphology were analyzed.
View Article and Find Full Text PDFIn the present communication, ZrTiO nanoparticles (NPs) are synthesized by the solution combustion method using urea (ZTOU) and oxalyl dihydrazide (ODH) (ZTODH) as fuel and calcined at 700 °C. The synthesized samples were characterized with different techniques. Powder X-ray diffraction studies show the presence of diffraction peaks corresponding to ZrTiO.
View Article and Find Full Text PDFUnlabelled: Sheath blight disease caused by Kuhn (teleomorph; ) is a major constraint in rice production. Among the different anastomosis groups (AGs) of , AG1-IA causes sheath blight of rice, which induce necrotic lesions on leaf sheaths of the infected plants. Several reports contradict the host specificity of anastomosis groups in .
View Article and Find Full Text PDFNanostructured NiO and Li-ion doped NiO have been synthesized via a facile microwave technique and simulated using the first principle method. The effects of microwaves on the morphology of the nanostructures have been studied by Field Emission Spectroscopy. X-ray diffraction studies confirm the nanosize of the particles and favoured orientations along the (111), (200) and (220) planes revealing the cubic structure.
View Article and Find Full Text PDFCr -doped Y O (0.5-9 mol%) was synthesized by a simple solution combustion method using Aloe vera gel as a fuel/surfactant. The final obtained product was calcined at 750°C for 3 h, which is the lowest temperature reported so far for the synthesis of this compound.
View Article and Find Full Text PDFGreen synthesis of multifunctional Zinc oxide nanoparticles (NPs) with a variety of morphologies were achieved by low temperature solution combustion route employing neem (Azadirachta indica) extract as fuel. The nanoparticles were characterized by PXRD, FTIR, XPS, Raman and UV-Visible spectroscopic studies. The Morphologies were studied by SEM and TEM analysis.
View Article and Find Full Text PDFSpectrochim Acta A Mol Biomol Spectrosc
September 2016
The study reports green mediated combustion route for the synthesis of Tb(3+) ion activated Y2O3 nanophosphors using Aloe Vera gel as fuel. The concentration of Tb(3+) plays a key role in controlling the morphology of Y2O3 nanostructures. The formation of different morphologies of Y2O3: Tb(3+) nanophosphors were characterized by PXRD, SEM, TEM and HRTEM.
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September 2016
MgO:Fe(3+) (0.1-5 mol%) nanoparticles (NPs) were synthesized via eco-friendly, inexpensive and simple low temperature solution combustion route using Aloe vera gel as fuel. The final products were characterized by SEM, TEM and HRTEM.
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September 2016
Facile and green route was employed for the synthesis of Y2O3:Dy(3+) (1-11 mol%) nanostructures (NSs) using Aloe vera gel as fuel. The formation of different morphologies of Y2O3:Dy(3+) NSs were characterized by SEM, TEM and HRTEM. PXRD data and Rietveld analysis evident the formation of single phase Y2O3 with cubic crystal structure.
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September 2016
Spherical shaped cerium dioxide (CeO2) nanoparticles (NPs) were synthesized via bio mediated route using Leucas aspera (LA) leaf extract. The NPs were characterized by PXRD, SEM, UV-Visible techniques. Photoluminescence (PL), photocatalysis and antibacterial properties of NPs were studied.
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June 2015
CeO2:Ho(3+) (1-9 mol%) nanopowders have been prepared by efficient and environmental friendly green combustion method using Aloe vera gel as fuel for the first time. The final products are well characterized by powder X-ray diffraction (PXRD), scanning electron microscopy (SEM), fourier transform infrared (FTIR). Bell, urchin, core shell and flower like morphologies are observed with different concentrations of the A.
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April 2015
We report the synthesis of Y2O3: Eu(3+) (1-11 mol%) nanoparticles (NPs) with different morphologies via eco-friendly, inexpensive and simple low temperature solution combustion method using Aloe Vera gel as fuel. The formation of different morphologies of Y2O3: Eu(3+) NPs were characterized by PXRD, SEM, TEM, HRTEM, UV-Visible and PL techniques. The PXRD data and Rietveld analysis confirms the formation of single phase Y2O3 with cubic crystal structure.
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April 2015
Mg2SiO4:Sm3+ (1-11 mol%) nanoparticles were prepared by a rapid low temperature solution combustion route. The powder X-ray diffraction (PXRD) patterns exhibit orthorhombic structure with α-phase. The average crystallite size estimated using Scherer's method, W-H plot and strain-size plots were found to be in the range 25-50 nm and the same was confirmed by Transmission Electron Microscopy (TEM).
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February 2015
The study involves preparation of samarium doped Y2SiO5 (YSO) nano powders by solution combustion method using urea as a fuel for the first time. Effect of different fluxes on the crystallization behavior, morphology and photoluminescence (PL) properties of YSO:Sm(3+) (1-9 mol%) were investigated. The final product was characterized by Powder X-ray diffraction (PXRD), Scanning Electron Microscopy (SEM) and UV-Vis spectroscopy.
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March 2015
A simple and low-cost solution combustion method was used to prepare Eu(3+) (1-11mol%) doped Zn2TiO4 nanophosphors at 500°C using zinc nitrates as precursors and oxalyl di-hydrazide (ODH) as fuel. The final product was calcined at 1100°C for 3h and then characterized by powder X-ray diffraction (PXRD), fourier transform infrared spectroscopy (FTIR), scanning electron microscopy (SEM), transmission electron microscopy (TEM) and UV-visible absorption (UV-Vis). The PXRD patterns of the sample calcined at 1100°C show pure cubic phase.
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January 2015
Novel crystalline tetragonal ZrO2: Eu(3+) phosphors were prepared by a facile and efficient low temperature solution combustion method at 400±10 °C using oxalyl dihydrazide (ODH) as fuel. The powder X-ray diffraction patterns and Rietveld confinement of as formed ZrO2: Eu(3+) (1-11 mol%) confirmed the presence of body centered tetragonal phase. The crystallite size estimated from Scherrer's and W-H plots was found to be in the range of 7-17 nm.
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December 2014
GdAlO3, GdAlO3:Eu(3+) and GdAlO3:Eu(3+):Bi(3+) nanophosphors were synthesised by solution combustion technique. Pure orthorhombic phase was obtained from powder X-ray diffraction (PXRD) studies. Scanning electron microscopy (SEM) micrographs showed the porous, agglomerated and irregular shaped particles.
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November 2014
Cobalt copper ferrite nanopowders with composition Co1-xCuxFe2O4 (0.0≤x≤0.5) was synthesized by solution combustion method.
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July 2014
CaTiO3:Sm(3+) (1-11 mol%) nanophosphors were successfully synthesized by a low temperature solution combustion method [LCS]. The structural and morphological properties of the phosphors were studied by using Powder X-ray diffractometer (PXRD), Fourier transform infrared (FTIR), X-ray photo electron spectroscopy (XPS), scanning electron microscope (SEM) and transmission electron microscopy (TEM). TEM studies indicate that the size of the phosphor is ∼20-35 nm.
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June 2014
Y(2)SiO(5) nanopowders are prepared by solution combustion method using DFH, sugar and urea as fuels. The final product was well characterized by powder X-ray diffraction, Scanning Electron Microscopy and UV-Vis spectroscopy. The average crystallite size was estimated using Debye-Scherer's formula and Williamson-Hall plots and are found to be in the range 34-40nm for DFH, 45-50nm for urea and 35-42nm for sugar respectively.
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September 2014
Nanoparticles of Eu(3+) doped (0-9 mol%) MgO were prepared using low temperature (400°C) solution combustion technique with metal nitrate as precursor and glycine as fuel. The powder X-ray diffraction (PXRD) patterns of the as-formed products show single cubic phase and no further calcination was required. The crystallite size was obtained using Scherer's formula and was found to be 5-6 nm.
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September 2014
Nanoparticles of Eu3+ doped (1-9 mol%) CaTiO3 were prepared using low temperature (500°C) solution combustion technique using metal nitrates as precursors and urea as fuel. The powder X-ray diffraction patterns of the as-formed products show single orthorhombic phase. The crystallite size was estimated using Scherrer's method and found to be in the range 40-45 nm.
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January 2014
Nanoparticles of magnesium oxide (MgO) have been prepared by low temperature solution combustion and hydrothermal method respectively. Powder X-ray diffraction (PXRD) patterns of MgO samples prepared by both the methods show cubic phase. The Scanning Electron Microscopy (SEM) studies reveal, the combustion derived product show highly porous, foamy and fluffy in nature than hydrothermally derived sample.
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