The paper presents the development of a rapid method for the direct determination of uranium using liquid scintillation analysis in uranium bearing materials with different uranium concentrations and with different impurity levels (U-ore, Uranium ore concentrate (UOC) and U-metal). Uranium extraction was carried out using hydrophobic ionic liquid Aliquat-336 thiosalicylate, ([A-336][TS]) from diluted samples in basic medium followed by liquid scintillation counting (LSC). Extraction efficiencies for uranium from aqueous medium was studied with very small volumes of ionic liquid under varying volume, pH and uranium concentration of the aqueous medium.
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