This paper deals with CFD analyses of the difference in the nature of the shock waves in supersonic flow under atmospheric pressure and pressure conditions at the boundary of continuum mechanics for electron microscopy. The first part describes the verification of the CFD analyses in combination with the experimental chamber results and the initial analyses using optical methods at low pressures on the boundary of continuum mechanics that were performed. The second part describes the analyses on an underexpanded nozzle performed to analyze the characteristics of normal shock waves in a pressure range from atmospheric pressure to pressures at the boundary of continuum mechanics.
View Article and Find Full Text PDFThe paper presents a methodology that combines experimental measurements and mathematical-physics analyses to investigate the flow behavior in a nozzle-equipped aperture associated with the solution of its impact on electron beam dispersion in an environmental scanning electron microscope (ESEM). The shape of the nozzle significantly influences the character of the supersonic flow beyond the aperture, especially the shape and type of shock waves, which are highly dense compared to the surrounding gas. These significantly affect the electron scattering, which influences the resulting image.
View Article and Find Full Text PDFThis paper describes the methodology of combining experimental measurements with mathematical-physics analyses in the investigation of flow in the aperture and nozzle. The aperture and nozzle separate the differentially pumped chamber from the specimen chamber in an environmental scanning electron microscope (ESEM). Experimental measurements are provided by temperature and pressure sensors that meet the demanding conditions of cryogenic temperature zones and low pressures.
View Article and Find Full Text PDFThis paper presents mathematical-physics analyses in the field of the influence of inserted sensors on the supersonic flow behind the nozzle. It evaluates differences in the flow in the area of atmospheric pressure and low pressure on the boundary of continuum mechanics. To analyze the formation of detached and conical shock waves and their distinct characteristics in atmospheric pressure and low pressure on the boundary of continuum mechanics, we conduct comparative analyses using two types of inserted sensors: flat end and tip.
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