Morphological Evolution of Sn-Metal-Based Anodes for Lithium-Ion Batteries Using Operando X-Ray Imaging.

Sn-based electrodes are promising candidates for next-generation lithium-ion batteries. However, it suffers from deleterious micro-structural deformation as it undergoes drastic volume changes upon lithium insertion and extraction. Progress in designing these materials is limited to complex structures.

Operando X-Ray Tomoscopy of Laser Beam Welding.

The phenomena occurring in a weld seam during advancement of a laser beam over a metallic component are still under dispute. The occurrence and evolution of porosity and the occasional blowout of melt need to be understood. Here, a recently developed X-ray tomoscopy setup is applied, providing one hundred 3D images per second to capture the temporal evolution of the melt pool in an AlSi9Cu3(Fe) die-casting while a laser beam advances.

Extrusion-based additive manufacturing of fungal-based composite materials using the tinder fungus Fomes fomentarius.

Background: Recent efforts in fungal biotechnology aim to develop new concepts and technologies that convert renewable plant biomass into innovative biomaterials. Hereby, plant substrates become metabolized by filamentous fungi to transform them into new fungal-based materials. Current research is thus focused on both understanding and optimizing the biology and genetics underlying filamentous fungal growth and on the development of new technologies to produce customized fungal-based materials.

Tomoscopy: Time-Resolved Tomography for Dynamic Processes in Materials.

The structure and constitution of opaque materials can be studied with X-ray imaging methods such as 3D tomography. To observe the dynamic evolution of their structure and the distribution of constituents, for example, during processing, heating, mechanical loading, etc., 3D imaging has to be fast enough.

An spatially resolved study of alkaline battery discharge using a novel hyperspectral detector and X-ray tomography.

An experimental technique is described for the collection of time-resolved X-ray diffraction information from a complete commercial battery cell during discharging or charging cycles. The technique uses an 80 × 80 pixel 2D energy-discriminating detector in a pinhole camera geometry which can be used with a polychromatic X-ray source. The concept was proved in a synchrotron X-ray study of commercial alkaline Zn-MnO AA size cells.

Fabrication and Characterization of Ice Templated Membrane Supports from Portland Cement.

Porous ceramic membranes for aqueous microfiltration and ultrafiltration processes suffer from the high-costs of material and processing. The latter is mainly due to the high-temperature sintering step. In this work, cement-based membrane supports from ultrafine Portland cement are studied as a low-cost alternative to traditional oxidic ceramic supports.

Using X-ray tomoscopy to explore the dynamics of foaming metal.

The complex flow of liquid metal in evolving metallic foams is still poorly understood due to difficulties in studying hot and opaque systems. We apply X-ray tomoscopy -the continuous acquisition of tomographic (3D) images- to clarify key dynamic phenomena in liquid aluminium foam such as nucleation and growth, bubble rearrangements, liquid retraction, coalescence and the rupture of films. Each phenomenon takes place on a typical timescale which we cover by obtaining 208 full tomograms per second over a period of up to one minute.

Simultaneous X-ray radioscopy/tomography and energy-dispersive diffraction applied to liquid aluminium alloy foams.

High-speed X-ray imaging in two dimensions (radioscopy) and three dimensions (tomography) is combined with fast X-ray diffraction in a new experimental setup at the synchrotron radiation source BESSY II. It allows for in situ studies of time-dependent phenomena in complex systems. As a first application, the foaming process of an aluminium alloy was studied in three different experiments.

Time-resolved in situ tomography for the analysis of evolving metal-foam granulates.

An experimental setup has been developed that allows for capturing up to 25 tomograms s using the white X-ray beam at the experimental station EDDI of BESSY II, Berlin, Germany. The key points are the use of a newly developed, precise and fast rotation stage, a very efficient scintillator and a fast CMOS camera. As a first application, the foaming of aluminium alloy granules at 923 K was investigated in situ.

Skinny emulsions take on granular matter.

Our understanding of the structural features of foams and emulsions has advanced significantly over the last 20 years. However, with a search for "super-stable" liquid dispersions, foam and emulsion science employs increasingly complex formulations which create solid-like visco-elastic layers at the bubble/drop surfaces. These lead to elastic, adhesive and frictional forces between bubbles/drops, impacting strongly how they pack and deform against each other, asking for an adaptation of the currently available structural description.