Publications by authors named "P Sanguino"

Solid-state and sol-gel procedures were used to prepare ZnAlCrO nanocrystal spinels. From the results obtained by X-ray diffraction (XRD) and transmission electron microscopy (TEM), it can be concluded that the samples prepared by sol-gel synthesis are better crystallized than the ones resulting from the solid-state method. Studies by spectroscopy of impedance were done in function of frequency (40-10 Hz) and temperature (540-680 K) in the sample prepared by sol-gel synthesis.

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Palygorskite is a natural fibrous clay mineral that can be used in several applications, for which colloidal stability in aqueous suspensions is a key point to improve its performance. In this study, methods of magnetic stirring, high-speed shearing, and ultrasonication, as well as different chemical dispersants, combined with these methods, namely carboxymethylcellulose, alginate, polyphosphate, and polyacrylate, were used to improve the dispersibility and the formation of stable suspensions of palygorskite in different conditions of pH. The stability and particle size of suspensions with a low concentration of palygorskite were evaluated by visual inspection, optical and electron microscopy, dynamic light scattering, and zeta potential measurements.

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The hexaferrite Ba Sr FeO compounds with = 0, 0.5 and 1 were synthesized by the autocombustion method. X-ray diffraction (XRD), Raman spectroscopy and transmission electron microscopy (TEM) were used for structural and morphological studies.

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