[Not Available].

The sample (< 1 mg) is burnt in an oxygen flask for the determination of rhenium. It is destroyed by a wet process in a Kjeldahl flask for the determination of rhodium or tellurium (sample <4-5 mg) or zirconium (sample <1.5 mg).

[Not Available].

The sample (up to 5 mg) is destroyed by using a wet process in a glass flask of the Kjeldahl type. Aluminium cobalt, tin and iron are determined spectrophotometrically. The following reactions are used: complexation of aluminium by Alizarin Red S and calcium cobalt(II) by tiron tin(IV) by phenylfluorone, iron(III) by tiron.