Under hydrothermal condition, kenaf cellulose carbamate (KCC) was synthesized using urea and kenaf core pulp (KCP) without catalyst and organic solvent. The KCC was prepared with various urea/KCP ratios (2:1, to 4:1 and 6:1) with the aid of autoclave and oil bath, whereas the regenerated KCC membranes were formed via solution casting method. The physical and thermal properties of KCC were studied.
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