The Electrochemical sensor based on carbon-clay paste electrode (CCPE) was constructed for sensitive determination of Tetracycline (Tc). The mineralogical composition, morphology, structure and performance of CCPE were characterized using X-ray diffraction powder, Fourier transform infrared spectroscopy (FTIR), Scanning electron microscopy (SEM) and Cyclic Voltammetry analysis. The CCPE is constituted of two types of clay having the ratio 1/1 and 2/1 characteristic of kaolinite and montmorillonite clay respectively.
View Article and Find Full Text PDFIn this work, a cyclic voltammetry analysis for the detection of Ascorbic Acid (AA) based on a carbon-clay paste electrode modified with titanium dioxide (CPEA/TiO) is presented. The electrochemical sensor was prepared using clay and carbon graphite, mixed with TiO to investigate the electrode behavior towards the detection of AA. Comprehensive characterization approaches including X-ray diffraction (XRD), Selected area electron diffraction (SAED), Transmission electron microscopy (TEM), Fourier transform infra-red spectroscopy (FTIR) were carried out on different samples.
View Article and Find Full Text PDFCalcinated and acidified clay modified carbon graphite electrode was deployed in the simultaneous evaluation of traces of Pb and Cd in solution. After 5 minutes of accumulation in the circuit, the sensitivity of the electrode was evaluated in a solution of NaSO (0.1 M) by square wave voltammetry on the one hand with Pb (II) and on the other hand with Cd (II).
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