Materials (Basel)
February 2024
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View Article and Find Full Text PDFA new mesoporous ZnMAlO photocatalyst was prepared using the metal-chitosan complexation method with different degrees of Zn cation substitution with cobalt and nickel ions (M = Co and Ni). Characterization using X-ray diffraction (XRD), Infrared absorption spectrometry (FTIR), energy dispersion spectroscopy (EDS), diffuse reflectance spectrometry (DRS), scanning electron miscoscopy (SEM), transmission electron miscroscopy (TEM), N adsorption- desorption isotherms using the Barrett-Joyner-Halenda (BJH) method, thermogravimetric analysis (TG) and differential thermal analysis (DTA) confirmed the formation of the spinel phase and high purity for all samples. N adsorption/desorption and size pore distribution confirmed the high surface area.
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