Advanced ionic conductors are crucial for a large variety of contemporary technologies spanning solid state ion batteries, fuel cells, gas sensors, water desalination, . In this work, we report on a new member of KTiOPO-structured materials, NaGaPOF, with sodium-ion conductivity. NaGaPOF has been obtained for the first time a facile two-step synthesis consisting of a hydrothermal preparation of an ammonia-based precursor, NHGaPOF, followed by an ion exchange reaction with NaNO.
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