Advances in machine learning (ML) have led to applications in safety-critical domains, including security, defense, and healthcare. These ML models are confronted with dynamically changing and actively hostile conditions characteristic of real-world applications, requiring systems incorporating ML to be reliable and resilient. Many studies propose techniques to improve the robustness of ML algorithms.
View Article and Find Full Text PDFIn this paper, a dual wavelength short near-infrared system is described for the detection of glucose levels. The system aims to improve the accuracy of blood glucose detection in a cost-effective and non-invasive way. The accuracy of the method is evaluated using real-time samples collected with the reference finger prick glucose device.
View Article and Find Full Text PDFAim: The aim of the study was to develop microbial enrichments from the nitrifying microbial consortia and the environment for simultaneous removal of ammonia, nitrate, and sulfide in aquaculture systems at varied salinities.
Methods And Results: Sulfur and nitrogen metabolites are the major factors affecting the farmed aquatic animal species and deteriorate the receiving environments causing ecological damage. The present study reports the development of microbial enrichments from the nitrifying microbial consortia and the environment.
Nearly 90% of cases of coccydynia can be managed with conservative medical treatment; the remaining 10% need other invasive modalities for pain relief, such as ganglion impar block (GIB) or radiofrequency ablation (RFA) of the ganglion impar. A systematic research was conducted of PubMed, MEDLINE, and Google Scholar to identify studies reporting pain relief in terms of visual analogue scale (VAS), or its counterparts, following GIB or RFA in coccydynia patients with the purpose to determine the efficacy of GIB and RFA of the ganglion impar in controlling pain in coccydynia patients. Seven studies were delineated, with a total of 189 patients (104 in GIB group and 85 in RFA group).
View Article and Find Full Text PDFUnderstanding of pesticide persistence and diffusion on the fresh vegetables are extremely important in food safety and decontamination process. In this study, we examine the persistence and diffusion behaviour of chlorpyrifos pesticide in five different species of vegetables. The chlorpyrifos pesticide was spiked on the vegetable surfaces and the extracted samples from peel and tissues were subjected to Gas Chromatography equipped with a Flame Photometric Detector (GC-FPD).
View Article and Find Full Text PDFNitrogen species such as ammonia and nitrite are considered as major stressors in modern aquaculture practices. We developed enrichments of ammonia oxidising bacteria (AOB) and nitrite oxidising bacteria (NOB) for effective mitigation of nitrogenous wastes in the shrimp culture operations. The objective of this study was to understand the microbial community composition of AOB and NOB enrichments using the V3-V4 region of the 16S rDNA gene by Illumina MiSeq sequencing.
View Article and Find Full Text PDFJ Food Sci Technol
September 2015
Coffee is known throughout the world for its distinct aroma and flavour which results from a number of volatile compounds present in it. It is very difficult to arrest the aromatic compounds once the roasting process is complete and it becomes even more challenging to store the beans for a longer time with the retained volatiles as these compounds are easily lost during industrialized processing such as the grinding of roasted coffee beans and storage of ground coffee. Thus, an attempt was made to minimise the loss of volatile from roasted coffee beans by coating with Carboxymethyl cellulose (CMC), Hydroxypropylmethyl cellulose (HPMC) and Whey protein concentrate.
View Article and Find Full Text PDFTwo chiral Mn complexes synthesized and characterized by single-crystal X-ray diffraction were grafted onto mesoporous silica MCM-41. The MCM-41-immobilized solid chiral catalysts were characterized by various spectrochemical and physicochemical methods (XRD, FTIR, Si NMR, TGA, UV/Vis/DRS, EPR, cyclic voltammetry, SEM, BET). Both the homogeneous and heterogeneous Mn chiral complexes are found to be effective catalysts for epoxidation of styrene.
View Article and Find Full Text PDFSynthesis of substituted 1,2-dihydropyridinones is described in a one pot reaction of β-enaminones and acetylene dicarboxylates where new C-C and C-N bonds were formed. The title compounds were obtained in moderate to good yields.
View Article and Find Full Text PDFEnviron Sci Pollut Res Int
May 2015
The coffee processing industry is one of the major agro-based industries contributing significantly in international and national growth. Coffee fruits are processed by two methods, wet and dry process. In wet processing, coffee fruits generate enormous quantities of high strength wastewater requiring systematic treatment prior to disposal.
View Article and Find Full Text PDFJ Food Sci Technol
December 2010
Pea-berry grade of green coffee (Coffea arabica) beans were roasted in a laboratory model spouted bed roaster at different temperatures (150-250°C) and times (30-300 s). The roasted samples were analysed for instrumental colour (hue, chroma and brightness) and texture. Brightness of the roasted samples varied between 5.
View Article and Find Full Text PDFA capillary electrophoresis (CE) and a high performance liquid chromatography (HPLC) method are described for the simultaneous determination of ethylenediaminetetraacetic acid (EDTA), S,S'-ethylenediaminedisuccinic acid (EDDS) and R,S-iminodisuccinic acid (IDS) complexing agents as their Fe(III) complexes in cosmetics like shower cream and foam bath. The non-biodegradable EDTA is used in combination with biodegradable analogues like EDDS and IDS in many commercial products. The HPLC method involves separation by reversed-phase ion pair chromatography on a C(18) column using methanol-formate buffer (20 mM tetrabutylammonium hydrogen sulfate, 15 mM sodium formate adjusted to pH 4.
View Article and Find Full Text PDFA capillary electrophoresis (CE) method is described for the simultaneous determination of copper and iron after complexation with a readily biodegradable chelating agent, [S,S']-ethylenediaminedisuccinic acid (EDDS), in wood pulp. CE separation was performed in a fused-silica capillary (50 microm i.d.
View Article and Find Full Text PDFA simple and rapid reversed-phase high-performance liquid chromatographic method for separation and determination of process-related impurities of difloxacin (DFL) was developed. The separation was achieved on a reversed-phase C(18) column using methanol-water-acetic acid (78:21.9:0.
View Article and Find Full Text PDFA simple and rapid high performance liquid chromatographic method for the separation and determination of synthetic impurities of norfloxacin was developed. The separation was achieved on a reversed-phase C(18) column using 0.01 M potassium dihydrogen orthophosphate and acetonitrile (60:40, v/v, pH 3.
View Article and Find Full Text PDFJ Pharm Biomed Anal
October 2003
An extensive survey of the literature published in various analytical and pharmaceutical chemistry related journals has been conducted and the high-performance liquid chromatography (HPLC) methods which were developed and used for determination of process-related impurities in drugs have been reviewed. This review covers the time period from 1995 to 2001 during which around 450 analytical methods including all types of chromatographic and hyphenated techniques were reported. HPLC with UV detection was found to be the technique of choice for many workers and more than 200 methods were developed using LC-UV alone.
View Article and Find Full Text PDFA simple and rapid high-performance liquid chromatographic method for the separation and determination of process-related impurities of sildenafil was developed. The separation was achieved on a reversed-phase C18 column using acetonitrile-0.05 M potassium dihydrogen orthophosphate (70:30 v/v) as a mobile solvent at a flow rate of 1.
View Article and Find Full Text PDFSimple, specific and rapid reversed-phase high-performance liquid chromatographic methods to separate and determine potential impurities of anthelmintic drugs viz., mebendazole, fenbendazole and albendazole are reported. These methods afforded efficient separation, good resolution and identification of all the impurities examined.
View Article and Find Full Text PDFThis study is aimed at evaluating the efficacy of the Ayurvedic system, especially for chronic diseases. Assessment of the subjective relief feed back was done on the lines as suggested in Caraka Samhita, one of the oldest classical Ayurvedic texts. An inter-disciplinary research work involving ancient medical learning and hi-tech modern electronic data processing unit evaluate the efficacy of the Ayurvedic treatment in a closed community.
View Article and Find Full Text PDFThe authors attempts to present in this paper different treatments employed for Sodhana with different and its toxicity reduction level.
View Article and Find Full Text PDFVanga bhasma, a popular Ayurvedic Medicine is prepared from Tin metal. This drug is claimed to have 'Sukrala' (Semenaugmentator), 'vrsya' (good for testis) properties in the literature and is widely in vogue for genito - urinary disorders in Ayurvedic practice. An experimental evaluation of the claim has been undertaken and the results have been presented in this paper.
View Article and Find Full Text PDFVangabhasma is a popular and effective dosage form prepared from tin metal in Ayurvedic practice. Since modern literature attributes certain toxicity to tin salts, an attempt is made to screen the acute and sub-acute toxicity of Vangabhasma in the form, dose and route as is in the practice or Ayurveda. In this paper, dose-effect relation of Vangabhasma on Digestive system (G.
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