Novel hybrid nanocomposites based on polyaniline (PANi), hydrolyzed pectin (HPEc) and CdS nanoparticles (NPs) as electrochemiluminescent biomaterials were prepared. The samples were fabricated heterogeneous chemical polymerization and studied by FTIR, XRD, SEM, EDX, UV/Vis, TGA and DMTA analyses. The CdS@HPEc--PANi nanocomposite was produced coprecipitation of CdS NPs by direct addition of aqueous cadmium nitrate and sodium sulfide solutions into the polymerization system containing PANi and HPEc.
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